Crystal structure of 2-cyano-1-methyl-pyridinium perchlorate

被引：1
|
作者：
Nguyen, Vu D. [1 ]
McCormick, Cameron A. [1 ]
Mague, Joel T. [2 ]
Koplitz, Lynn V. [1 ]
机构：
[1] Loyola Univ, Dept Chem, New Orleans, LA 70118 USA
[2] Tulane Univ, Dept Chem, New Orleans, LA 70118 USA
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
关键词：
crystal structure; salt; pyridinium; perchlorate; hydrogen bonding;
D O I：
10.1107/S2056989015019155
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title salt, C7H7N2+center dot ClO4-, comprises two independent formula units. The solid-state structure comprises corrugated layers of cations and of anions, approximately parallel to (010). The supramolecular layers are stabilized and connected by C-H center dot center dot center dot O hydrogen bonding to consolidate a three-dimensional architecture. A close pyridinium-perchlorate N center dot center dot center dot O contact [2.867 (5) angstrom] is noted. The crystal was refined as an inversion twin.
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收藏
页码：O852 / U448
页数：9
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