HEADSPACE ANALYSIS OF 1,4-DIOXANE IN PRODUCTS CONTAINING POLYETHOXYLATED SURFACTANTS BY GC-MS

被引：25
|
作者：
RASTOGI, SC
机构：
[1] National Environmental Research Institute, Division of Environmental Chemistry, Ministry of Environment, Søborg, DK-2860
来源：
CHROMATOGRAPHIA | 1990年 / 29卷 / 9-10期
关键词：
1,4-dioxane; Gas chromatography-mass spectrometry; Headspace analysis; Polyethoxylated surfactants;
D O I：
10.1007/BF02261391
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A headspace, gas chromatography-mass spectrometric (GC-MS) method for the identification and quantitation of 1,4-dioxane in polyethoxylated surfactants is described. An isotope dilution method employing 1,4-d8-dioxane has been used for the quantitation of 1,4-dioxane which is based on the determination of the molecular ion (mass 88) by MS. The detection limit of the method was 0.3 ppm 1,4-dioxane. 82% of the cosmetic products investigated were found to contain 0.3-96 ppm 1,4-dioxane, and 85% of the products for dish washing investigated contained 1.8-65 ppm 1,4-dioxane. © 1990 Friedr. Vieweg & Sohn Verlagsgesellschaft mbH.
引用
收藏
页码：441 / 445
页数：5
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