SYNTHESIS OF NOVEL UNSYMMETRICAL MONOAMINATED PHTHALOCYANINES

被引：70

作者：

SASTRE, A

TORRES, T

HANACK, M

机构：

[1] UNIV AUTONOMA MADRID, FAC CIENCIAS, DEPT QUIM ORGAN C1, E-28049 MADRID, SPAIN

[2] UNIV TUBINGEN, LEHRSTUHL ORGAN CHEM 2, INST ORGAN CHEM, D-72076 TUBINGEN, GERMANY

来源：

TETRAHEDRON LETTERS | 1995年 / 36卷 / 46期

关键词：

D O I：

10.1016/0040-4039(95)01781-C

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Metal-free monoaminophthalocyanine 3 was synthesised by reacting of subphthalocyanine 1 with 5-amino-1,3-diiminoisoindoline 2. Alternatively, compound 3 was prepared from octadecylaminodiiminoisoindoline 6 by reaction with 1 to give 7 followed by acidic hydrolisis. The zinc complex 8 was obtained from 3 by treatment with anhydrous zinc acetate. The preparation of 8 by template condensation of subphthalocyanine 1 with aminodiiminoisoindoline 2 and zinc acetate was unsuccessful. In this case, a mixture of statistical distribution compounds was obtained. A tentative reaction pathway for the condensation between subphthalocyanines and diiminoisoindolines is also given.

引用

页码：8501 / 8504

页数：4

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