(E)-1-{4-[Bis(4-bromophenyl)methyl]-piperazin-1-yl}-3-(4-methylphenyl)prop-2-en-1-one

被引：0
|
作者：
Zhong, Yan [1 ]
Zhang, XiaoPing [2 ]
Wu, Bin [3 ]
机构：
[1] Southeast Univ, Sch Chem & Chem Engn, Nanjing 210096, Jiangsu, Peoples R China
[2] Nanjing Med Univ, Ctr Lab Anim, Nanjing 210029, Jiangsu, Peoples R China
[3] Nanjing Med Univ, Sch Pharm, Hanzhong Rd 140, Nanjing 210029, Jiangsu, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
data-to-parameter ratio = 15.4; mean σ(C-C) = 0.012 Å; R factor = 0.075; single-crystal X-ray study; T = 293 K; wR factor = 0.155;
D O I：
10.1107/S1600536812003820
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C 27H 26Br 2N 2O, the piperazine ring adopts a chair conformation with the N - C bonds in equatorial orientations. The C=C double bond has an E configuration. The dihedral angle between the bromobenzene rings is 83.0 (4)°. In the crystal, inversion dimers linked through pairs of C - H⋯O hydrogen bonds generate R 2 2(10) loops.
引用
收藏
页码：O605 / U1423
页数：9
相关论文
共 50 条
  • [41] 1-(4-bromophenyl)-3-(3-methoxyphenyl)prop-2-en-1-one
    Patil, P. S.
    Chantrapromma, Suchada
    Fun, Hoong-Kun
    Dharmaprakash, S. M.
    Babu, H. B. Ramesh
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2612 - U1193
  • [42] 1-(4-bromophenyl)-3-(2-thienyl)prop-2-en-1-one
    Patil, P. S.
    Ng, Shea-Lin
    Razak, Ibrahim Abdul
    Fun, Hoong-Kun
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3718 - O3720
  • [43] 3-(4-methylphenyl)-1-(2-naphthyl)prop-2-en-1-one
    Moorthi, SS
    Chinnakali, K
    Nanjundan, S
    Balaji, R
    Fun, HK
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3885 - O3887
  • [44] 1-(4-Bromophenyl)-3-(2,4,5-trimethoxyphenyl)prop-2-en-1-one
    Patil, P. S.
    Rosli, Mohd Mustaqim
    Fun, Hoong-Kun
    Razak, Ibrahim Abdul
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4644 - O4645
  • [45] 3-(4-Methylphenyl)-1-(2-pyrrolyl)prop-2-en-1-one
    Gong, Zhen-Qi
    Shen, You-Liang
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3939 - U1980
  • [46] 1-(4-Methylphenyl)-3-(2-thienyl)prop-2-en-1-one
    Rosli, Mohd Mustaqim
    Patil, P. S.
    Fun, Hoong-Kun
    Razak, Ibrahim Abdul
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4648 - O4649
  • [47] (E)-3-(4-Bromophenyl)-1-(3,4-dichlorophenyl)prop-2-en-1-one
    Kant, Rajni
    Kamni
    Narayana, B.
    Veena, K.
    Yathirajan, H. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O836 - U2679
  • [48] The 0.893/0.104/0.003 cocrystal of 1-(4-methylphenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one, 3-(3-chloro-4,5-dimethoxyphenyl)-1-(4-methylphenyl)prop-2-en-1-one and 3-(3,5-dichloro-4-methoxyphenyl)-1-(4-methylphenyl)prop-2-en-1-one
    Ng, Shea-Lin
    Razak, Ibrahim Abdul
    Fun, Hoong-Kun
    Patil, P. S.
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4650 - O4652
  • [49] 1-(2-Hydroxy-4-methoxyphenyl)-3-(4-methylphenyl)prop-2-en-1-one
    Thippeswamy, G. B.
    Kumar, D. Vijay
    Jayashree, B. S.
    Sridhar, M. A.
    Prasad, J. Shashidhara
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O829 - U78
  • [50] (2E)-3-(4-Bromophenyl)-1-(2-methyl-4phenyl-3-quinolyl)prop-2-en-1-one
    Prasath, R.
    Sarveswari, S.
    Vijayakumar, V.
    Narasimhamurthy, T.
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1110 - U406
12345