Synthesis and X-ray Diffraction Study of Radium Plumbate

被引：2
|
作者：
Butkalyuk, P. S. [1 ]
Butkalyuk, I. L. [1 ]
Kuznetsov, R. A. [1 ]
Tomilin, S. V. [1 ]
机构：
[1] Publ Joint Stock Co, State Sci Ctr, Res Inst Atom Reactors, Dimitrovgrad 10, Ulyanovsk 433510, Ulyanovsk Oblas, Russia
来源：
RADIOCHEMISTRY | 2013年 / 55卷 / 01期
关键词：
alpha emitters; radium-226; plumbates; platinates;
D O I：
10.1134/S1066362213010086
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Previously unknown mixed oxide RaPbO3 was prepared by thermal decomposition of a mixture of radium and lead carbonates. An X-ray diffraction study showed that radium plumbate crystallizes in the cubic perovskite structural type. The unit cell parameter (a = 4.303 angstrom) and crystallographic density (rho = 10.42 g cm(-3)) were determined. Formation of a new compound, RaPtO3-x, upon sintering of mixtures of radium and lead carbonates at 800 degrees C in a platinum crucible was detected. A similar barium compound can be formed upon calcination of barium compounds in platinum vessels in air.
引用
收藏
页码：41 / 45
页数：5
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