EXPERIMENTS DIRECTED TOWARDS THE SYNTHESIS OF ANTHRACYCLINONES .14. AN INTERMEDIATE FOR THE SYNTHESIS OF VINEOMYCINS

被引：15

作者：

CAMBIE, RC ^{[1
]}

HOWE, TA ^{[1
]}

PAUSLER, MG ^{[1
]}

RUTLEDGE, PS ^{[1
]}

WOODGATE, PD ^{[1
]}

机构：

[1] UNIV AUCKLAND, DEPT CHEM, AUCKLAND, NEW ZEALAND

来源：

AUSTRALIAN JOURNAL OF CHEMISTRY | 1987年 / 40卷 / 06期

关键词：

D O I：

10.1071/CH9871063

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Anthrarufin (4) has been converted by a high-yielding route involving sequential reductive Claisen rearrangements into 1-acetoxy-5-methoxy-9,10-dioxo-6-(2''-oxopropyl)-9,10-dihydroanthracene-2-carbaldehyde (3), an intermediate which is suitable for the synthesis of vineomycins. The thermal Claisen rearrangements of some allyl ethers of 1,5-dihydroxyanthraquinone have been examined.

引用

页码：1063 / 1072

页数：10

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