Crystal structure of 4-(4-methoxypheny1)-4 ',4 '-dimethy1-3-p-tolyl-3 ',4 '-dihydro-1 ' H,3H-spiro[isoxazole-5,2 '-naphthalen]-1 '-one

被引:0
|
作者
Akhazzane, Mohamed [1 ]
Al Houari, Ghali [1 ]
El Yazidi, Mohamed [1 ]
Saadi, Mohamed [2 ]
El Ammari, Lahcen [2 ]
机构
[1] Univ Sidi Mohammed Ben Abdellah, Fac Sci Dhar el Mahraz, Lab Chim Organ, Fes, Morocco
[2] Univ Mohammed V Rabat, Fac Sci, Lab Chim Solide Appl, Rabat, Morocco
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
关键词
crystal structure; isoxazole; tetralone;
D O I
10.1107/S2056989015022033
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C28H27NO3, the cyclohexanone and isoxazole rings have envelope conformations, with the methylene and spiro C atoms as the flaps, respectively. The mean plane of the isoxazole ring is inclined slightly to the p-tolyl ring, making a dihedral angle of 14.20 (9)degrees, and is nearly perpendicular to the mean plane through the tetralone moiety and to the methoxyphenyl ring [dihedral angles = 83.41 (8) and 72.12 (9)degrees, respectively]. The crystal packing is stabilized mainly by van der Waals forces.
引用
收藏
页码:O981 / U877
页数:8
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