1-(6-Fluoro-1,3-benzothiazol-2-yl)-2-(1-phenylethylidene)hydrazine

被引：0
|
作者：
Fun, Hoong-Kun [1 ]
Quah, Ching Kheng [1 ]
Munirajasekhar, D. [2 ]
Himaja, M. [2 ]
Sarojini, B. K. [3 ]
机构：
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia
[2] VIT Univ, Sch Adv Sci, Chem Div, Vellore 632014, Tamil Nadu, India
[3] PA Coll Engn, Dept Chem, Mangalore 574153, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
D O I：
10.1107/S1600536812030851
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title compound, C15H12FN3S, consists of two independent molecules with comparable geometries. In one molecule, the 1,3-benzothiazole ring system (r.m.s. deviation = 0.011 angstrom) forms a dihedral angle of 19.86 (6)degrees with the phenyl ring. The corresponding r.m.s. deviation and dihedral angle for the other molecule are 0.014 angstrom and 22.32 (6)degrees, respectively. In the crystal, molecules are linked via N-H center dot center dot center dot N, C-H center dot center dot center dot F and C-H center dot center dot center dot N hydrogen bonds into a three-dimensional network. The crystal studied was a non-merohedral twin with a refined BASF value of 0.301 (2).
引用
收藏
页码：02438 / +
页数：11
相关论文
共 50 条
  • [41] Bis[2-(1,3-benzothiazol-2-yl)phenolato-O,N]chlorooxorhenium(V)- dichloromethane (1/1.5)
    Panneerselvam, Kaliyamoorthy
    Lu, Tian-Huey
    Tung, Shu-Fang
    Chattopadhyay, Pabitra
    Lo, Jem-Mau
    Chung, Chung-Sun
    Acta Crystallographica, Section C: Crystal Structure Communications, 1999, 55 (11): : 1802 - 1804
  • [42] Polymorphism of bis(1,3-benzothiazol-2-yl) trithio-carbonate
    Kafuta, Kevin
    Golz, Christopher
    Alcarazo, Manuel
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2020, 76 : 1126 - +
  • [43] CRYSTAL AND MOLECULAR-STRUCTURE OF 2-(1,3-BENZOTHIAZOL-2-YL)-2-(4-TERT-BUTYLCYCLOHEXYLIDENE)ETHANONITRILE
    WU, F
    LI, YJ
    COX, O
    HERNANDEZ, WJ
    JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH, 1993, 23 (08): : 645 - 648
  • [44] Bis[2-(1,3-benzothiazol-2-yl)phenolato-O,N]chlorooxorhenium(V)-dichloromethane (1/1.5)
    Panneerselvam, K
    Lu, TH
    Tung, SF
    Chattopadhyay, P
    Lo, JM
    Chung, CS
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 1802 - 1804
  • [45] 1,1,2,2-Tetrakis(1,3-benzothiazol-2-yl)ethene chloroform disolvate
    Hagos, Tesfamariam K.
    Nogai, Stefan D.
    Dobrzanska, Liliana
    Cronje, Stephanie
    Raubenheimer, Helgard G.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2378 - U904
  • [46] Diethyl [4-(1,3-benzothiazol-2-yl)benzyl]phosphonate
    Peng, Rong
    Li, Huisheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O3236 - U1243
  • [47] [(1,3-Benzothiazol-2-yl)aminocarbonyl]methyl piperidine-1-carbodithioate monohydrate
    Lu, Xu-Jia
    Zhao, Hong-Bin
    Chen, Liang
    Yang, De-Liang
    Wang, Bang-Ying
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1488 - U1325
  • [48] 2-(5-Chloro-1,3-benzothiazol-2-yl)-4-methoxyphenol
    Yousuf, Sammer
    Shah, Shazia
    Ambreen, Nida
    Khan, Khalid M.
    Ahmad, Shakil
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2877 - +
  • [49] Dimethyl 3-acetyl-3-(1,3-benzothiazol-2-yl)pentanedioate
    Baryala, Yamna
    Salem, Moussa
    Essassi, El Mokhtar
    Reuter, Hans
    Izaaryene, Maher
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2290 - U1871
  • [50] N-(1,3-benzothiazol-2-yl)-4-(dimethylamino)-benzylamine
    Saraçoglu, H
    Çaliskan, N
    Davran, C
    Soylu, S
    Bati, H
    Büyükgüngör, O
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O2090 - O2092
12345