INCLUSION COMPOUND OF THIOUREA WITH AMINES

被引：0
|
作者：
YUTRONIC, N
GONZALEZ, G
JARA, P
机构：
来源：
BOLETIN DE LA SOCIEDAD CHILENA DE QUIMICA | 1992年 / 37卷 / 01期
关键词：
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The inclusion of some heterocyclic amines in thiourea leads to following host-guest compounds: bis(thiourea)-hexamethylenetetramine), hexaquis(thiourea)-(dicyclohexilamine), tris(thiourea)-(1-bicyclo[2,2,2]octane), tris(thiourea)-(N-methylcyclohexilamine), pentaquis(thiourea)-bis(3-azabicyclo[3,2,2]nonane). Characterization of the products by melting point determination, elemental analysis, IR. H-1-NMR and mass spectroscopy confirm the inclusion process. Powder X-ray diffraction analysis indicates the products are crystalline compounds in the rhombohedral space group R3c.
引用
收藏
页码：39 / 42
页数：4
相关论文
共 50 条
  • [41] 35Cl NQR study of incommensurate state in thiourea-hexachloroethane inclusion compound
    Panich, AM
    Semenov, AR
    Chekhova, GN
    Krieger, JH
    Goren, SD
    SOLID STATE COMMUNICATIONS, 1999, 110 (07) : 363 - 367
  • [42] A study of out-of-plane cation dynamics in a bis-thiourea pyridinium chloride inclusion compound
    Pajzderska, A.
    Czarnecki, P.
    Embs, J. P.
    Gonzalez, M. A.
    Juranyi, F.
    Krawczyk, J.
    Peplinska, B.
    Wasicki, J.
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2011, 13 (19) : 8908 - 8914
  • [43] Molecular dynamics of guest molecules in the cyclohexane/thiourea inclusion compound: a combined MD-IQNS study
    Jones, MJ
    Camus, S
    Guillaume, F
    Harris, KDM
    Dianoux, AJ
    PHYSICA B, 1997, 241 : 472 - 474
  • [44] A high resolution quasielastic neutron scattering study of the guest molecules dynamics in the cyclohexane/thiourea inclusion compound
    Desmedt, A
    Guillaume, F
    Combet, J
    Dianoux, AJ
    PHYSICA B, 2001, 301 (1-2): : 59 - 64
  • [45] Aminomethylation of Thiourea with Formaldehyde and Cyclic Amines
    Martinovich, Yu. A.
    Ramsh, S. M.
    Hamoud, F.
    Fundamenskii, V. S.
    Gurzhii, V. V.
    Zakharov, V. I.
    Khrabrova, E. S.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2018, 54 (06) : 878 - 885
  • [46] Aminomethylation of Thiourea with Formaldehyde and Cyclic Amines
    Yu. A. Martinovich
    S. M. Ramsh
    F. Hamoud
    V. S. Fundamenskii
    V. V. Gurzhii
    V. I. Zakharov
    E. S. Khrabrova
    Russian Journal of Organic Chemistry, 2018, 54 : 878 - 885
  • [47] ADAMANTANE INCLUSION COMPLEXES WITH THIOUREA AND SELENOUREA
    GOPAL, R
    ROBERTSON, BE
    RUTHERFORD, JS
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1989, 45 : 257 - 259
  • [48] DYNAMICS OF FERROCENE IN A THIOUREA INCLUSION MATRIX
    LOWERY, MD
    WITTEBORT, RJ
    SORAI, M
    HENDRICKSON, DN
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1990, 112 (11) : 4214 - 4225
  • [49] IRA and 13C-NMR spectral properties of the layered inclusion compound bis(thiourea)hexamethylenetetramine.
    Jara, P
    González, G
    Manríquez, V
    Wittke, O
    Yutronic, N
    JOURNAL OF THE CHILEAN CHEMICAL SOCIETY, 2004, 49 (01): : 39 - 43
  • [50] Molecular dynamics of cyclohexane guest molecules in the cyclohexane/thiourea inclusion compound: an incoherent quasielastic neutron scattering investigation
    Jones, MJ
    Guillaume, F
    Harris, KDM
    Aliev, AE
    Girard, P
    Dianoux, AJ
    MOLECULAR PHYSICS, 1998, 93 (04) : 545 - 554
12345