A TETRAAZAMACROCYCLE FUNCTIONALIZED WITH PENDANT PYRAZOLE GROUPS - SYNTHESIS OF THE OCTADENTATE LIGAND 1,4,7,10-TETRAKIS(1-PYRAZOLYLMETHYL)-1,4,7,10-TETRAAZACYCLODODECANE (L) AND ITS TRANSFORMATION TO THE LIGAND 1,4,7-TRIS(1-PYRAZOLYLMETHYL)-10-((ETHYLOXY)METHYL)-1,4,7,10-TETRAAZACYCLODODECANE (L') - STRUCTURAL CHARACTERIZATIONS OF THE COMPLEXES [NIL]I2, [NIL'](BPH4)2.2(CH3)2CO, AND [ZNL'](BPH4)2.(CH3)2CO

被引：0

作者：

NORANTE, GD ^{[1
]}

DIVAIRA, M ^{[1
]}

MANI, F ^{[1
]}

MAZZI, S ^{[1
]}

STOPPIONI, P ^{[1
]}

机构：

[1] UNIV FIRENZE,DIPARTIMENTO CHIM,VIA MARAGLIANO 77,I-50144 FLORENCE,ITALY

来源：

INORGANIC CHEMISTRY | 1990年 / 29卷 / 15期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

引用

页码：2822 / 2829

页数：8

共 44 条

[31] STRUCTURAL STUDIES ON METAL-COMPLEXES OF CHIRAL CYCLEN .3. THE STRUCTURE OF CHLORO[(2R,5S,8R,11S)-1,4,7,10-TETRABENZYL-2,5,8,11-TETRAETHYL-1,4,7,10-TETRAAZACYCLODODECANE]COPPER(II) CHLORIDE CHLOROFORM SOLVATE
KOBAYASHI, K
SAKURAI, T
HASEGAWA, A
TSUBOYAMA, S
TSUBOYAMA, K
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1982, 38 (APR): : 1154 - 1158
[32] THERMODYNAMIC, KINETIC, AND STRUCTURAL STUDY OF THE LIGATIONAL PROPERTIES OF THE MACROBICYCLIC AZA-LIGAND 4,7,10,17,23-PENTAMETHYL-1,4,7,10,13,17,23-HEPTAAZABICYCLO[11.7.5]PENTACOSANE (L1) AND OF ITS MACROCYCLIC PRECURSOR 1,4,7,13-TETRAMETHYL-1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE (L2) - CRYSTAL-STRUCTURE OF [ZN(L1)(H2O)](BPH4)2
BENCINI, A
BIANCHI, A
DAPPORTO, P
FUSI, V
GARCIAESPANA, E
MICHELONI, M
PAOLETTI, P
PAOLI, P
RODRIGUEZ, A
VALTANCOLI, B
INORGANIC CHEMISTRY, 1993, 32 (12) : 2753 - 2760
[33] SYNTHESIS, CHARACTERIZATION, AND 1/T(1) NMRD PROFILES OF GADOLINIUM(III) COMPLEXES OF MONOAMIDE DERIVATIVES OF DOTA-LIKE LIGANDS - X-RAY STRUCTURE OF THE 10-[2-[[2-HYDROXY-1-(HYDROXYMETHYL)ETHYL]AMINO]-1-[(PHENYLMETHOXY)METHYL]-2-OXO-ETHYL]-1,4,7,10-TETRAAZACYCLODODECANE-1,4,7-TRIACETIC ACID GADOLINIUM(III) COMPLEX
AIME, S
ANELLI, PL
BOTTA, M
FEDELI, F
GRANDI, M
PAOLI, P
UGGERI, F
INORGANIC CHEMISTRY, 1992, 31 (12) : 2422 - 2428
[34] MERCURY MACROCYCLIC COMPLEXES - SYNTHESIS AND CRYSTAL-STRUCTURES OF ([HGCL(MU-CL)(L1)][HG(MU-CL)2])N (L1 = 1,4,7,10-TETRAOXA-13-AZACYCLOPENTADECANE), [HG(L2)CL2] (L2 = 1,4,7,10,13-PENTAOXA-16-AZACYCLOOCTADECANE) AND [HG(L3)CL2] (L3 = 16-METHYL-1,4,7,10,13-PENTAOXA-16-AZACYCLOOCTADECANE)
BYRIEL, KA
DUNSTER, KR
GAHAN, LR
KENNARD, CHL
LATTEN, JL
INORGANICA CHIMICA ACTA, 1992, 196 (01) : 35 - 41
[35] STRUCTURAL STUDIES ON METAL-COMPLEXES OF CHIRAL CYCLEN .5. CHLORO[(2RS,5RS,8RS,11SR)-1,4,7,10-TETRABENZYL-2,5,8,11-TETRAETHYL-1,4,7,10-TETRAAZACYCLODODECANE]COPPER(II) DICHLOROCUPRATE(I) ETHANOL SOLVATE, [CUCL(C44H60N4)]- [CUCL2].3C2H6O
TSUBOYAMA, S
KOBAYASHI, K
SAKURAI, T
TSUBOYAMA, K
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1984, 40 (JUL) : 1178 - 1181
[36] Metal ion interactions with nucleobases in the tetradentate 1,4,7,10-tetraazacyclododecane (cyclen)-ligand system: Crystal structures of [Cu(cyclen)(adeninato)]•ClO4•2H2O, [{Cu(cyclen)}2(hypoxanthinato)]•(ClO4)3, [Cu(cyclen)(theophyllinato)]3•(ClO4)3•2H2O, and [Cu(cyclen) (xanthinato)]•(0.7ClO4)•(0.3ClO4)•3H2O•(0.5H2O)3
Rahman, Md. Shahidur
Yuan, Hou Qun
Kikuchi, Takanori
Fujisawa, Ikuhide
Aoki, Katsuyuki
JOURNAL OF MOLECULAR STRUCTURE, 2010, 966 (1-3) : 92 - 101
[37] Synthesis, crystal structures and thermal decomposition of two novel supramolecular complexes [Ni(cyclen)(H2O)2] (tpa) and [Cu(cyclen)H2O](tpa)•3H2O (Cyclen=1,4,7,10-tetraazacyclododecane, tpa=dianion of terephalic acid)
Ren, YW
Li, J
Zhao, SM
Zhang, FX
STRUCTURAL CHEMISTRY, 2005, 16 (04) : 439 - 444
[38] Coordination studies of the ligand series RNH•CO•(CH2)n•CO•NHR where R = alkyl, aryl; O = O, S and n = 0,1,2.: Part 6.: Crystal structures and bonding considerations of the ligands MeNH•CO•CH2•CO•NHMe (L1), MeNH•CO•CH2•CH2•CO•NHMe (L4), MeNH•CS•CH2•CS•NHMe (L5) and the SnIV complexes SnBr4L1•L1, SnBr4L2•2THF and SnBr4L3•MeCN where L2 = iC3H7NH•CO•CH2•CO•NHiC3H7 and L3 = iC3H7NH•CS•CH2•CS•NHiC3H7
Willey, GR
Baker, RJ
Haslop, JV
Spry, MP
Drew, MGB
POLYHEDRON, 1998, 17 (19) : 3291 - 3303
[39] Structure of the double salt [Co-II(Cl)L(3)]Cl-[Co-III(CO3)L3]Cl[L(3) (2R,5R,8R,11R)-1,7-dibenzyl-2,5,8,11-tetraethyl-1,4,7,10-tetraazacyclododecane) and related species
Tsuboyama, S
Fujimoto, J
Hanabira, S
Yasuda, N
Kobayashi, K
Sakurai, T
Tsuboyama, K
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1996, (01): : 45 - 51
[40] TRANSITION-METAL COMPLEXES WITH SULFUR LIGANDS .26. REGIOSPECIFIC TEMPLATE ALKYLATION OF [FE-II(CO)2] CENTERS - SYNTHESIS AND STRUCTURE OF THE IRON(II) COMPLEX [FEL1L2(TBU4-DTTD)] WITH THE STERICALLY-DEMANDING TETRADENTATE THIOETHER-THIOLATE LIGAND TBU4-DTTD2- = (TETRA-T-BUTYL)-2,3-8,9-DIBENZO-1,4,7,10-TETRATHIADECANE(2-) - (L1 = L2 = CO, PME3, LI = CO, L2 = PME3, PPH3)E
SELLMANN, D
FREYBERGER, G
EBERLEIN, R
BOHLEN, E
HUTTNER, G
ZSOLNAI, L
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1987, 323 (01) : 21 - 35

← 1 2 3 4 5 →