MASS-SPECTRAL FRAGMENTATION PATHWAYS IN NITRAMINES - A COLLISION-INDUCED DISSOCIATION STUDY

被引：10
|
作者：
YINON, J [1 ]
BRUMLEY, WC [1 ]
BRILIS, GM [1 ]
BULUSU, S [1 ]
机构：
[1] USA,ARMAMENT RES,CTR DEV & ENGN,DIV ENERGET MAT,PICATINNY ARSENAL,NJ 07806
来源：
ORGANIC MASS SPECTROMETRY | 1990年 / 25卷 / 01期
关键词：
D O I：
10.1002/oms.1210250105
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A collision‐induced dissociation (CID) study of five synthesized nitramines was carried out using a hybrid EBQQ mass spectrometer. CID spectra were obtained in two modes: B/E linked‐scan mode and MS/MS mode using the EB sector combination as the first mass spectrometer and the QQ as collision cell and second mass spectrometer, respectively. Fragmentation pathways of the compounds were determined in the electron‐impact mode. It was found that dominant fragmentation pathways included the loss of OH, NO2 and HNO2 in addition to the loss of CH2NNO and CH2NNO2. Copyright © 1990 John Wiley & Sons, Ltd.
引用
收藏
页码：14 / 20
页数：7
相关论文
共 50 条
  • [21] Collision-induced dissociation mass spectra of glucosinolate anions
    Bialecki, Jason B.
    Ruzicka, Josef
    Weisbecker, Carl S.
    Haribal, Meena
    Attygalle, Athula B.
    JOURNAL OF MASS SPECTROMETRY, 2010, 45 (03): : 272 - 283
  • [22] Fragmentation study of peptide acetals and aldehydes using in-source collision-induced dissociation
    Buré, C
    Le Falher, G
    Lange, C
    Delmas, A
    JOURNAL OF MASS SPECTROMETRY, 2004, 39 (07): : 817 - 823
  • [23] THE MASS-SPECTRAL FRAGMENTATION OF ISOXAZOLYLDIHYDROPYRIDINES
    KNERR, G
    MCKENNA, JI
    QUINCY, DA
    NATALE, NR
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1987, 24 (05) : 1429 - 1433
  • [24] Structural study of spirolide marine toxins by mass spectrometryPart I. Fragmentation pathways of 13-desmethyl spirolide C by collision-induced dissociation and infrared multiphoton dissociation mass spectrometry
    Lekha Sleno
    Anthony J Windust
    Dietrich A Volmer
    Analytical and Bioanalytical Chemistry, 2004, 378 : 969 - 976
  • [25] Fragmentation study of iridoid glucosides through positive and negative electrospray ionization, collision-induced dissociation and tandem mass spectrometry
    Es-Safi, Nour-Eddine
    Kerhoas, Lucien
    Ducrot, Paul-Henri
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2007, 21 (07) : 1165 - 1175
  • [26] Collision-induced dissociation of peptide thioesters:: the influence of peptide length on fragmentation
    Buré, C
    Boujard, O
    Bertrand, M
    Lange, C
    Delmas, AF
    EUROPEAN JOURNAL OF MASS SPECTROMETRY, 2005, 11 (01) : 31 - 34
  • [27] A comprehensive study on rearrangement reactions in collision-induced dissociation mass spectrometric fragmentation of protonated diphenyl and phenyl pyridyl ethers
    Baira, Shandilya Mahamuni
    Ragampeta, Srinivas
    Talluri, M. V. N. Kumar
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2019, 33 (18) : 1440 - 1448
  • [28] Electron-Activated Dissociation and Collision-Induced Dissociation Glycopeptide Fragmentation for Improved Glycoproteomics
    Macauslane, Kyle L.
    Pegg, Cassandra L.
    Nouwens, Amanda S.
    Kerr, Edward D.
    Seitanidou, Joy
    Schulz, Benjamin L.
    ANALYTICAL CHEMISTRY, 2024, : 10986 - 10994
  • [29] Predicting collision-induced dissociation mass spectra: understanding the role of the mobile proton in small molecule fragmentation
    Wright, Patricia
    Alex, Alexander
    Pullen, Frank
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2016, 30 (09) : 1163 - 1175
  • [30] Study of mass spectrometric fragmentations of tributyl phosphate via collision-induced dissociation
    Lesage, D
    Virelizier, H
    Tabet, JC
    Jankowski, CK
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2001, 15 (20) : 1947 - 1956
12345