Practical Synthesis of Di-tert-Butyl-Phosphinoferrocene

被引：5

作者：

Busacca, Carl A. ^{[1
]}

Eriksson, Magnus C. ^{[1
]}

Haddad, Nizar ^{[1
]}

Han, Z. Steve ^{[1
]}

Lorenz, Jon C. ^{[1
]}

Qu, Bo ^{[1
]}

Zeng, Xingzhong ^{[1
]}

Senanayake, Chris H. ^{[1
]}

Reeves, Corey M. ^{[1
]}

Stoltz, Brian M. ^{[1
]}

机构：

[1] Boehringer Ingelheim Pharmaceut Inc, Chem Dev Dept, POB 368, Ridgefield, CT 06877 USA

来源：

ORGANIC SYNTHESES | 2013年 / 90卷

关键词：

D O I：

10.15227/orgsyn.090.0316

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Caution! tert-Butylithium is extremely pyrophoric and must not be allowed to come into contact with the atmosphere. This reagent should only be handled by individuals trained in its proper and safe use. It is recommended that transfers be carried out by using a 20-mL or smaller glass syringe filled to no more than 2/3 capacity or by cannula. For a discussion of procedures for handling air-sensitive reagents, see Aldrich Technical Bulletin AL-134.

引用

页码：316 / 326

页数：11

共 50 条

[21] Synthesis of thienylhydrogermanes and their transformations in the presence of di(tert-butyl) peroxide
Lukevics E.
Pudova O.A.
Mazheika I.
Grinberga S.
Chemistry of Heterocyclic Compounds, 1997, 33 (2) : 171 - 174
[22] DI-TERT-BUTYL DICARBONATE
POPE, BM
YAMAMOTO, Y
TARBELL, DS
ORGANIC SYNTHESES, 1988, 50-9 : 418 - 421
[23] BROMINATION OF 1,4-DI-TERT BUTYLBENZENE - SYNTHESIS OF 1,4-DI-TERT BUTYL-2-BROMOBENZENE AND SOME TERT BUTYL-DIBROMOBENZENES
BAAS, JMA
WEPSTER, BM
RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS, 1966, 85 (05): : 457 - &
[24] Di-tert-butyl Azodicarboxylate
Dias Pires, Marina J.
SYNLETT, 2012, (11) : 1701 - 1702
[25] DI-TERT-BUTYL THIOKETONE
OHNO, A
NAKAMURA, K
NAKAZIMA, Y
OKA, S
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1975, 48 (08) : 2403 - 2404
[26] DI-TERT-BUTYL-DI-AMINOALKYL SILICATES
DIGIORGIO, PA
SOMMER, LH
WHITMORE, FC
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1949, 71 (09) : 3254 - 3256
[27] SYNTHESIS AND THERMAL-DECOMPOSITION OF DI-TERT-BUTYL PEROXYDICARBONATE
KOMAI, T
MATSUYAMA, K
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1985, 58 (08) : 2207 - 2211
[28] Dehydration of methyl-di-tert.-butyl-carbinol. Fission and isomerisation of di-tert.-butyl-ethylene.
Nasarow, IN
BERICHTE DER DEUTSCHEN CHEMISCHEN GESELLSCHAFT, 1936, 69 : 18 - 21
[29] IMPROVED SYNTHESIS OF 2,6-DI-TERT-BUTYL-4-METHYLPYRYLIUM CHLOROSTANNATE AND PERCHLORATE AND OF 2,6-DI-TERT-BUTYL-4-METHYLPYRIDINE
BALABAN, AT
ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1977, 9 (3-5) : 125 - 130
[30] REACTIONS OF ALKENES WITH DI-TERT-BUTYL PEROXIDE AND TERT-BUTYL PEROXYPIVALATE
SHELTON, JR
UZELMEIE.CW
JOURNAL OF ORGANIC CHEMISTRY, 1970, 35 (05): : 1576 - &

← 1 2 3 4 5 →