Practical Synthesis of Di-tert-Butyl-Phosphinoferrocene

被引：5
|
作者：
Busacca, Carl A. [1 ]
Eriksson, Magnus C. [1 ]
Haddad, Nizar [1 ]
Han, Z. Steve [1 ]
Lorenz, Jon C. [1 ]
Qu, Bo [1 ]
Zeng, Xingzhong [1 ]
Senanayake, Chris H. [1 ]
Reeves, Corey M. [1 ]
Stoltz, Brian M. [1 ]
机构：
[1] Boehringer Ingelheim Pharmaceut Inc, Chem Dev Dept, POB 368, Ridgefield, CT 06877 USA
来源：
ORGANIC SYNTHESES | 2013年 / 90卷
关键词：
D O I：
10.15227/orgsyn.090.0316
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Caution! tert-Butylithium is extremely pyrophoric and must not be allowed to come into contact with the atmosphere. This reagent should only be handled by individuals trained in its proper and safe use. It is recommended that transfers be carried out by using a 20-mL or smaller glass syringe filled to no more than 2/3 capacity or by cannula. For a discussion of procedures for handling air-sensitive reagents, see Aldrich Technical Bulletin AL-134.
引用
收藏
页码：316 / 326
页数：11
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