STRUCTURE DETERMINATION OF A TRILAYER MISFIT COMPOUND (GD-EPSILON-SN1-EPSILON-S)(1.16)(NBS2)(3)

被引:19
|
作者
HOISTAD, LM
MEERSCHAUT, A
BONNEAU, P
ROUXEL, J
机构
[1] Institut des Matériaux de Nantes, UMR-CNRS 110, Laboratoire de Chimie des Solides, 44072 Nantes Cedex 02
关键词
D O I
10.1006/jssc.1995.1066
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
We present the synthesis, single crystal refinement, and powder refinement of a new misfit compound, (GdepsilonSn1-epsilonS)(1.16)(NbS2)(3). The single crystal structure was determined using a composite approach comprised of three refinement steps. The powder refinement was done using four-dimensional space with one modulation vector to model the incommensurate axis. The structure consists of three consecutive layers of NbS2 followed by a layer of MS, (C) 1995 Academic Press, Inc.
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页码:435 / 441
页数:7
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