Crystal structure of 2-cyclohexyl-1,3-thiazolo[4,5-b]pyridine

被引：1
|
作者：
El-Hiti, Gamal A. [1 ]
Smith, Keith [2 ]
Hegazy, Amany S. [2 ]
Ajarim, Mansour D. [3 ]
Kariuki, Benson M. [2 ]
机构：
[1] King Saud Univ, Dept Optometry, Coll Appl Med Sci, Cornea Res Chair, POB 10219, Riyadh 11433, Saudi Arabia
[2] Cardiff Univ, Sch Chem, Cardiff CF10 3AT, S Glam, Wales
[3] Minist Interior, Criminal Evidence, Riyadh 11632, Saudi Arabia
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
关键词：
crystal structure; cyclohexane; thiazolopyridine derivatives; thiazolo[4,5-b]pyridine;
D O I：
10.1107/S2056989015019106
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C12H14N2S, the cyclohexane ring adopts a chair conformation with the exocyclic C-C bond in an equatorial orientation. The mean plane through the cyclohexane ring (all atoms) is twisted from the thiazolopyridine ring system (r.m.s. deviation = 0.013 angstrom) by 39.57 (6)degrees. In the crystal, molecules form (100) sheets, although there are no specific directional interactions between them. The crystal stucture was refined as a two-component perfect twin.
引用
收藏
页码：O866 / +
页数：6
相关论文
共 50 条
  • [21] SYNTHESIS OF THIAZOLO[4,5-B]QUINOXALINE AND RELATED COMPOUNDS
    ISMAIL, IM
    SAUER, W
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1978, 16 (08): : 683 - 685
  • [22] 2-(3,5-Dimethyl-1H-pyrazol-1-yl)thiazolo[4,5-b]pyridine
    Lan, Honghong
    Zheng, Min
    Wang, Ye
    MOLBANK, 2019, 2019 (03)
  • [23] QUATERNIZATION OF 1H-IMIDAZO[4,5-B]PYRIDINE AND 4-METHYL-4H-IMIDAZO[4,5-B]PYRIDINE
    YUTILOV, YM
    IGNATENKO, AG
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1994, (09): : 1232 - 1233
  • [24] STRUCTURE OF 1-(2,4-DINITROPHENYL)IMIDAZO[4,5-B]PYRIDINE
    ESCANDE, A
    DUMAS, Y
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1980, 36 (MAY): : 1217 - 1218
  • [25] REGIOSELECTIVE SYNTHESIS OF 4-OXOBUTYLOXAZOLO[4,5-B]PYRIDINE-2-ONES AND 3-OXOBUTYLOXAZOLO[4,5-B]PYRIDINE-2-ONES AND THEIR DERIVATIVES
    PESHAKOVA, L
    KALCHEVA, V
    JOURNAL FUR PRAKTISCHE CHEMIE, 1991, 333 (01): : 183 - 186
  • [26] Synthesis and properties of 2-(2-furyl)[1,3]oxazolo[4,5-b]pyridine
    El'chaninov, M. M.
    Aleksandrov, A. A.
    Illenzeer, E. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2014, 50 (12) : 1826 - 1828
  • [27] Antitumor properties of thiazolo[4,5-b]pyridin-2-one derivatives
    Chaban, Taras
    Matiychuk, Vasyl
    Mahlovanyy, Anatoliy
    Chaban, Ihor
    Ogurtsov, Volodymyr
    Lelyukh, Maryan
    BIOINTERFACE RESEARCH IN APPLIED CHEMISTRY, 2020, 10 (04): : 5944 - 5950
  • [28] SYNTHESIS OF THIAZOLO(4,5-B)-QUINOXALINES AND RELATED-COMPOUNDS
    AMMAR, YA
    ISMAIL, IM
    ELSHARIEF, AMS
    MOHAMED, YA
    AMER, RM
    JOURNAL FUR PRAKTISCHE CHEMIE, 1988, 330 (03): : 421 - 427
  • [29] Synthesis and properties of 2-(2-furyl)[1,3]oxazolo[4,5-b]pyridine
    M. M. El’chaninov
    A. A. Aleksandrov
    E. V. Illenzeer
    Russian Journal of Organic Chemistry, 2014, 50 : 1826 - 1828
  • [30] 2,7-Dimethyl-1,3-thiazolo[4,5-d]pyridazin-4(5H)-one
    Al-Youbi, Abdulrahman O.
    Asiri, Abdullah M.
    Faidallah, Hassan M.
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2467 - U1481
12345