MASS-SPECTROMETRY AND LIQUID-CHROMATOGRAPHY - MASS-SPECTROMETRY OF ALPHA-AMINO BETA-NITROSTILBENES

被引：0
|
作者：
HAYESMAJSTOROVIC, J [1 ]
GUERNETNIVAUD, E [1 ]
GUERNET, M [1 ]
VIEL, C [1 ]
机构：
[1] FAC PHARM TOURS,PHARMACOCHIM PROD NAT & ANAL STRUCT,F-37042 TOURS,FRANCE
来源：
ANALYTICAL LETTERS | 1993年 / 26卷 / 10期
关键词：
(Z)-ALPHA-AMINO BETA-NITROSTILBENES; NITROENAMINES; HPLC; MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY MASS SPECTROMETRY;
D O I：
10.1080/00032719308017465
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
(Z)-alpha-amino beta-nitrostilbenes are obtained by the reaction of either ammonia or primary or secondary amines on (Z)-alpha, beta-dinitrostilbene (DNS). The fragmentometric study of these compounds by electron impact and chemical ionization was carried out. The conditions in which it may be possible to determine the purity of these compounds were obtained by HPLC on reversed phase. However the resolution factor between DNS and benzyl- or phenyl-aminonitroenamine is not sufficient for UV detection; only liquid chromatography-mass spectra coupling with negative ionization enables the detection of the possible presence of DNS in these nitro enamino derivatives.
引用
收藏
页码：2239 / 2249
页数：11
相关论文
共 50 条
  • [11] ELECTROSPRAY INTERFACE FOR LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY
    HIRAOKA, K
    KUDAKA, I
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1990, 4 (12) : 519 - 526
  • [12] 10 YEARS OF LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY
    ARPINO, PJ
    JOURNAL OF CHROMATOGRAPHY, 1985, 323 (01): : 3 - 11
  • [13] LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF VANADYL PORPHYRINS
    SUNDARARAMAN, P
    VESTAL, C
    ORGANIC GEOCHEMISTRY, 1993, 20 (07) : 1099 - 1104
  • [14] LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF DEXAMETHASONE AND BETAMETHASONE
    CAIRNS, T
    SIEGMUND, EG
    STAMP, JJ
    SKELLY, JP
    BIOMEDICAL MASS SPECTROMETRY, 1983, 10 (03): : 203 - 208
  • [15] LIQUID-CHROMATOGRAPHY AND MASS-SPECTROMETRY - DIFFICULT MARRIAGE
    ARPINO, P
    RECHERCHE, 1975, 6 (59): : 769 - 772
  • [16] ELECTROSPRAY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF GINSENOSIDES
    VANBREEMEN, RB
    HUANG, CR
    LU, ZZ
    RIMANDO, A
    FONG, HHS
    FITZLOFF, JF
    ANALYTICAL CHEMISTRY, 1995, 67 (21) : 3985 - 3989
  • [17] LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF ANTISENSE OLIGONUCLEOTIDES
    BOTHNER, B
    CHATMAN, K
    SARKISIAN, M
    SIUZDAK, G
    BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 1995, 5 (23) : 2863 - 2868
  • [18] AUTOMATED LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY FOR CHROMATOGRAPHERS
    PULLEN, FS
    RICHARDS, DS
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1995, 9 (02) : 188 - 190
  • [19] ELECTROSPRAY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY OF CAROTENOIDS
    VANBREEMEN, RB
    ANALYTICAL CHEMISTRY, 1995, 67 (13) : 2004 - 2009
  • [20] A BIBLIOGRAPHY OF COMBINED LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY
    EDMONDS, CG
    MCCLOSKEY, JA
    EDMONDS, VA
    BIOMEDICAL MASS SPECTROMETRY, 1983, 10 (04): : 237 - 252
12345