TRACE DETERMINATION OF VANADIUM AND NICKEL IN SAUDI-ARABIAN PETROLEUM AND PETROLEUM-PRODUCTS BY MICROEMULSION ICP-MS

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作者：

ALSWAIDAN, HM

机构：

来源：

ATOMIC SPECTROSCOPY | 1993年 / 14卷 / 06期

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O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

The combination of microemulsion sampling technique, standard addition method, and inductively coupled plasma-mass spectrometry (ICP-MS) has been applied for the determination of vanadium and nickel in Saudi Arabian petroleum and petroleum products. Detection limits of 2.52 mug/g V and 0.30 mug/g Ni in heavy crude oil samples were achieved. Recoveries of added metals as oil-soluble salts lie between 98-103%, and the relative standard deviation for five replicate samples was less than 5% in all cases.

引用

页码：170 / 173

页数：4

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