CERTIFIED REFERENCE MATERIALS FOR THE DETERMINATION OF CADMIUM IN POLYETHYLENE

被引:21
|
作者
PAUWELS, J [1 ]
LAMBERTY, A [1 ]
DEBIEVRE, P [1 ]
GROBECKER, KH [1 ]
BAUSPIESS, C [1 ]
机构
[1] MERCEDES BENZ AG,D-70322 STUTTGART,GERMANY
来源
关键词
D O I
10.1007/BF00322924
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Four polyethylene reference materials with cadmium concentrations in the range of 40 to 400 mg/kg have been certified by IRMM on behalf of Verband der Automobilindustrie e.V. (VDA), Frankfurt, Germany. The homogeneity of the materials was verified using Solid Sampling Zeeman Atomic Absorption Spectrometry (SS-ZAAS). Their cadmium content was determined by Isotope Dilution Mass Spectrometry (IDMS) using a quadrupole thermal ionization mass spectrometer. The certified uncertainties were about 3% relative and correspond to confidence levels of 95%; they take into account all contributions of statistical and systematic nature. The material was used within the scope of IRMM's International Measurement Evaluation Programme (IMEP).
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页码:409 / 411
页数:3
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