LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY STUDIES OF 9-FLUORENYLMETHYL CHLOROFORMATE DERIVATIVES OF POLYAMINES

被引：5
|
作者：
LU, Z [1 ]
VEENING, H [1 ]
COUTANT, JE [1 ]
机构：
[1] MERRELL DOW RES INST,CINCINNATI,OH 45215
来源：
JOURNAL OF CHROMATOGRAPHY | 1991年 / 540卷 / 1-2期
关键词：
D O I：
10.1016/S0021-9673(01)88809-9
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Liquid chromatography-mass spectrometry experiments were carried out to elucidate the structure of the carbamate derivatives formed when polyamines, such as ethylenediamine and putrescine, react with the precolumn fluorophore forming reagent, 9-fluorenylmethyl chloroformate. It has been shown that both primary amine functionalities derivatize with the reagent for polyamines.
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页码：199 / 206
页数：8
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