High-resolution adiabatic scanning calorimeter for small samples

被引：11

作者：

Schnelle, W

Gmelin, E

机构：

[1] Max-Planck-Institut für Festkörperforschung, D-70569 Stuttgart

来源：

THERMOCHIMICA ACTA | 1995年 / 269卷

关键词：

adiabatic scanning calorimetry; double calorimetry; high resolution calorimeter; small samples;

D O I：

10.1016/0040-6031(94)02666-1

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

An improved version of a low-temperature double calorimeter for the temperature range 20-320 K is presented. The temperature of the adiabatic shield is increased at a programmable rate, while the temperature differences to the samples are regulated to zero. Temperature control and data acquisition are achieved by software algorithms integrated in a single computer program. The apparatus yields a typical precision Delta C-p/C-p of 10(-3) with approximate to 50 data K-1.

引用

页码：27 / 32

页数：6

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