Four common techniques for the removal of dissolved oxygen from water have been examined: boiling at 1 atm, boiling under reduced pressure, purging with N2 and sonication under reduced pressure. After treatment, the residual oxygen in solution was analysed by the Winkler method. Nitrogen purging for 20-40 min at flow rate of 25 mL/s was found to be the most effective oxygen removal method. Boiling at 1 atm was found to be the least effective. None of the techniques evaluated here lead to complete removal of oxygen. The concentration of residual dissolved oxygen after purging for 20-40 minutes with nitrogen is 0.2-0.4 ppm.
机构:
ENERGY MINES & RESOURCES CANADA,CANMET,PHY MET RES LABS,OTTAWA,ONTARIO,CANADAENERGY MINES & RESOURCES CANADA,CANMET,PHY MET RES LABS,OTTAWA,ONTARIO,CANADA
MALAIYANDI, M
SASTRI, VS
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ENERGY MINES & RESOURCES CANADA,CANMET,PHY MET RES LABS,OTTAWA,ONTARIO,CANADAENERGY MINES & RESOURCES CANADA,CANMET,PHY MET RES LABS,OTTAWA,ONTARIO,CANADA