AUTOMATIC SAMPLER FOR CURIE-POINT PYROLYSIS-GAS CHROMATOGRAPHY WITH ON-COLUMN INTRODUCTION OF PYROLYSATES

被引:5
|
作者
FISCHER, WG
KUSCH, P
机构
[1] Fischer Labor- und Verfahrenstechnik GmbH, Industriepark Kottenforst
来源
JOURNAL OF CHROMATOGRAPHY | 1990年 / 518卷 / 01期
关键词
D O I
10.1016/S0021-9673(01)93158-9
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An automatic sampler for Curie-point pyrolysis-gas chromatography (GC) to be used in connection with a packed GC column for direct (on-column) introduction of pyrolysates is described. A comparison with the conventional method for pyrolysate introduction with the on-column method is given. Good reproducibility of the results obtained for poly(acrylonitrile-co-1,3-butadiene-co-styrene-co-α-methyl-styrene) and poly(methyl methacrylate) pyrolysis products was observed (relative standard deviation <5%). Examples of other applications are presented. © 1990.
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页码:9 / 19
页数:11
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