HIGH-RESOLUTION GAS-CHROMATOGRAPHY - MASS-SPECTRAL ANALYSIS OF CARBOHYDRATES USING METHOXYOXIME ACETATES

被引：7
|
作者：
HERDERICH, M [1 ]
SCHREIER, P [1 ]
机构：
[1] UNIV WURZBURG, LEHRSTUHL LEBENSMITTELCHEM, W-8700 WURZBURG, GERMANY
来源：
PHYTOCHEMICAL ANALYSIS | 1993年 / 4卷 / 06期
关键词：
METHOXYOXIME ACETATES; CARBOHYDRATE ANALYSIS; HIGH RESOLUTION GAS CHROMATOGRAPHY MASS SPECTROSCOPY; DERIVATIZATION;
D O I：
10.1002/pca.2800040603
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Methoxyoxime acetates of carbohydrates and partially methylated derivatives were easily separated by high resolution gas chromatography (HRGC) and showed characteristic mass spectra (MS). Thus, the conversion of carbohydrates to the corresponding methoxyoxime acetates offers an attractive derivatization for subsequent HRGC and HRGC/MS analysis of carbohydrates, particularly in glycoconjugates of plant origin.
引用
收藏
页码：256 / 260
页数：5
相关论文
共 50 条
  • [1] MULTIDIMENSIONAL GAS-CHROMATOGRAPHY WITH INFRARED AND MASS-SPECTRAL DETECTION
    KROCK, KA
    WILKINS, CL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 209 : 4 - ANYL
  • [2] THE ANALYSIS OF WAXES AND GREASES USING HIGH-RESOLUTION GAS-CHROMATOGRAPHY
    GILES, JJ
    JOURNAL OF THE FORENSIC SCIENCE SOCIETY, 1987, 27 (04): : 231 - 239
  • [3] HIGH-RESOLUTION GAS-CHROMATOGRAPHY IN THE ANALYSIS OF RESIDUES
    NETO, FRDA
    QUIMICA NOVA, 1995, 18 (01): : 65 - 67
  • [4] DETERMINATION OF CARBOHYDRATES AS ALDITOL ACETATES BY GAS-CHROMATOGRAPHY
    VIDAL, T
    PASTOR, JFC
    TAPPI JOURNAL, 1984, 67 (09): : 132 - 132
  • [5] ANALYSIS OF INSECT PHEROMONES BY QUADRUPOLE MASS FRAGMENTOGRAPHY AND HIGH-RESOLUTION GAS-CHROMATOGRAPHY
    BUSER, HR
    ARN, H
    JOURNAL OF CHROMATOGRAPHY, 1975, 106 (01): : 83 - 95
  • [6] ANALYSIS OF DINITROFLUORANTHENES BY HIGH-RESOLUTION CAPILLARY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY
    RAMDAHL, T
    AREY, J
    ZIELINSKA, B
    ATKINSON, R
    WINER, AM
    JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1986, 9 (09): : 515 - 517
  • [7] GAS-CHROMATOGRAPHY - MASS-SPECTRAL TECHNIQUES IN CITRUS ESSENCE RESEARCH
    NAGY, S
    KLIM, M
    FOOD TECHNOLOGY, 1986, 40 (11) : 95 - &
  • [8] ANALYSIS OF VOLATILE COMPONENTS IN JUNIPER OIL BY HIGH-RESOLUTION GAS-CHROMATOGRAPHY AND COMBINED GAS-CHROMATOGRAPHY MASS-SPECTROMETRY
    BONAGA, G
    GALLETTI, GC
    ANNALI DI CHIMICA, 1985, 75 (3-4) : 131 - 136
  • [9] ANALYSIS OF LEGUME OLIGOSACCHARIDES BY HIGH-RESOLUTION GAS-CHROMATOGRAPHY
    KAROUTIS, AI
    TYLER, RT
    SLATER, GP
    JOURNAL OF CHROMATOGRAPHY, 1992, 623 (01): : 186 - 190
  • [10] HIGH-RESOLUTION SUBTRACTIVE GAS-CHROMATOGRAPHY
    GELSOMINI, N
    JOURNAL OF CHROMATOGRAPHY, 1983, 279 (NOV): : 473 - 475
12345