HETEROGENEOUS CATALYTIC SYNTHESIS AND STRUCTURE OF 5,5A,10A,11-TETRAHYDRO-10H-INDENO[1,2-B]QUINOLINE

被引：2

作者：

PLESHAKOV, VG ^{[1
]}

AMBACHEU, KD ^{[1
]}

RYASHENTSEVA, MA ^{[1
]}

SERGEEVA, ND ^{[1
]}

VENER, MV ^{[1
]}

MURUGOVA, LA ^{[1
]}

ZVOLINSKY, OV ^{[1
]}

PROSTAKOV, NS ^{[1
]}

机构：

[1] RUSSIAN ACAD SCI,ND ZELINSKII ORGAN CHEM INST,MOSCOW 117913,RUSSIA

来源：

RUSSIAN CHEMICAL BULLETIN | 1994年 / 43卷 / 06期

关键词：

10H-INDENO[1,2-B]QUINOLINE; HYDROGENATION; RHENIUM HEPTASULFIDE; 5,5A,10A,11-TETRAHYDRO-10H-INDENO[1,2-B; STEREOCHEMISTRY; MOLECULAR MECHANICS CALCULATIONS; PC MODEL PROGRAM;

D O I：

10.1007/BF01558074

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Hydrogenation of 10H-indeno[1,2-b]quinoline in benzene in the presence of R(2)S(7) (250 degrees C, pH(2) = 140 atm, 4 h) gave 5,5a,10a,11-tetrahydro-10H-indeno[1,2-b]quinoline, the structure of which was established by mass-, IR, UV, C-13, and H-1 NMR spectra. The cis fusion of the indan and tetrahydroquinoline fragments, the axial orientation of the proton at C(5a), and the equatorial orientation of the proton at C(10a) were confirmed by molecular mechanics calculations using the PC MODEL program.

引用

页码：1037 / 1040

页数：4

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