2,3-DI-TERT-BUTYL-1-TELLURADIPHOSPHIRANE AND RELATED PHOSPHORUS TELLURIUM HETEROCYCLES

被引：17
|
作者：
DUMONT, WW
SEVERENGIZ, T
机构：
[1] Institut für Anorganische und Analytische Chemie, Technischen Universität Hagenring, Braunschweig
[2] Braunschweig
来源：
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 1993年 / 619卷 / 06期
关键词：
PHOSPHORUS-TELLURIUM HETEROCYCLES; 2,3-DI-TERT-BUTYL-1-TELLURADIPHOSPHIRANE;
D O I：
10.1002/zaac.19936190619
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
2,3-Di-tert-butyl-1-telluradiphosphirane was isolated in pure state by trap to trap condensation after reaction of 1,2-Di-tert-butyl-1,2-dichlorodiphosphane with sodium telluride in pentane suspension. The telluradiphosphirane and other P-Te heterocycles (t-BuP)(n)Te(m) (n = 2, m = 1; n = 3, m = 1,2; n = 4, m = 1,2) are formed from 1,2-Di-tert-butyl-1,2-dichlorodiphosphane or tert-butyldichlorophosphane with bis(trimethylsilyl)telluride and from the reaction of tert-butylbis(trimethylsilyl)phosphane with elemental tellurium. The proposed structures of the P-Te heterocycles are based on P-31- and Te-125-n.m.r. and MS data
引用
收藏
页码：1083 / 1087
页数：5
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