Synthesis and structure of 2,4,6,8-tetramethyl-3,7-dithia-2,4,6,8-tetraazabicyclo[3.3.0]octane 3,3,7,7-tetraoxide

被引:0
|
作者
G. A. Gazieva
K. A. Lysenko
A. N. Kravchenko
O. V. Lebedev
机构
[1] Russian Academy of Sciences,Zelinskii Institute of Organic Chemistry
[2] Russian Academy of Sciences,Nesmeyanov Institute of Organometallic Compounds
来源
关键词
Octane; Glyoxal; Unshared Electron Pair; Sulfonyl Group; Glycoluril;
D O I
暂无
中图分类号
学科分类号
摘要
Condensation of N,N′-dimethylsulfamide with glyoxal gave 2,4,6,8-tetramethyl-3,7-dithia-2,4,6,8-tetraazabicyclo[3.3.0]octane 3,3,7,7-tetraoxide, a sulfur-containing analog of 2,4,6,8-tetramethyl-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione (Mebicar). The product structure was studied by X-ray analysis.
引用
收藏
页码:1715 / 1718
页数:3
相关论文
共 50 条
  • [1] Synthesis and structure of 2,4,6,8-tetramethyl-3,7-dithia-2,4,6,8-tetraazabicyclo[3.3.0]octane 3,3,7,7-tetraoxide
    Gazieva, G. A.
    Lysenko, K. A.
    Kravchenko, A. N.
    Lebedev, O. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 43 (11) : 1715 - 1718
  • [2] Successful synthesis of 2,4,6,8-tetraiodo-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione
    Yagovkin, YA
    Bakibaev, AA
    Bystritsky, EL
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1995, (12): : 1695 - 1696
  • [3] Synthesis of sulfoanalogs of 2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-diones
    Gazieva G.A.
    Kravchenko A.N.
    Lebedev O.V.
    Abelentsev V.I.
    Pharmaceutical Chemistry Journal, 2001, 35 (2) : 72 - 74
  • [4] Studies of Quantum Chemistry of Structure and Properties of 3,7-Bis (nitroimino)-2,4,6,8-tetranitro-2,4,6,8-tetraazabicyclo [3.3.0]octane
    Jin Xing-Hui
    Hu Bing-Cheng
    Jia Huan-Qing
    Lu Chun-Xu
    CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 2013, 34 (07): : 1685 - 1690
  • [5] New Synthesis of 2,4,6,8-Tetramethyl-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione Using Etidronic Acid as a “Green” Catalyst
    S. Yu. Panshina
    O. V. Ponomarenko
    A. A. Bakibaev
    V. S. Malkov
    Russian Journal of Organic Chemistry, 2020, 56 : 2067 - 2073
  • [6] Synthesis of 2-monofunctionalized 2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-diones
    Kravchenko, AN
    Maksareva, EY
    Belyakov, PA
    Sigachev, AS
    Chegaev, KY
    Lyssenko, KA
    Lebedev, OV
    Makhova, NN
    RUSSIAN CHEMICAL BULLETIN, 2003, 52 (01) : 192 - 197
  • [7] Synthesis of 2-monofunctionalized 2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-diones
    A. N. Kravchenko
    E. Yu. Maksareva
    P. A. Belyakov
    A. S. Sigachev
    K. Yu. Chegaev
    K. A. Lyssenko
    O. V. Lebedev
    N. N. Makhova
    Russian Chemical Bulletin, 2003, 52 : 192 - 197
  • [8] Spectroscopic study of the complexation of iodine with 2,4,6,8-tetraphenyl-2,4,6,8-tetraazabicyclo[3.3.0]octane
    Rouhollahi, A
    Kakanejadifard, A
    Farnia, SMF
    Shamsipur, M
    POLISH JOURNAL OF CHEMISTRY, 1997, 71 (06) : 731 - 738
  • [10] Crystal Structure and Properties of 7-Imino-3-Nitroimino-2,4,6,8-Tetraazabicyclo[3.3.0]Octane Hydrochloride
    Jin, Xinghui
    Hu, Bingcheng
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2016, 642 (9-10): : 635 - 642