共 3 条
Synthesis and Characterization of Amino-Terminated Chloration Modified Peanut Shell and Its Application to Preconcentrate and Detect the Concentration of Sunset Yellow in Drink and Jelly Samples
被引:0
|作者:
Baohong Lin
Song Li
Lei Fang
Minliang Zhu
Chunhua Xiong
机构:
[1] Zhejiang Gongshang University,Department of Applied Chemistry
[2] Tufts University,Department of Infectious Disease and Global Health
来源:
Food Analytical Methods
|
2018年
/
11卷
关键词:
Peanut shell;
Adsorption;
Hyper-branched polymers;
Fruit juice;
Jelly;
D O I:
暂无
中图分类号:
学科分类号:
摘要:
Sunset yellow, as a common pigment, is harmful to people’s health. In this work, a new sensitive adsorbent based on the chlorination peanut shell and HBP-NH2 was fabricated via one-step synthesis. Optimization of the modified peanut shell was carried out at different temperatures, different molar ratios of reagents, and different time intervals in HBP-NH2 using Response Surface Methodology (RSM) for the first attempt. The structure of modified peanut shell was characterized by FT-IR, SEM, and TGA analysis. The adsorption properties of the modified peanut shell for Sunset yellow were investigated by batch and column experiments. Batch adsorption’s results suggested that modified peanut shell had a high adsorption capability for Sunset yellow and its maximum saturated adsorption capacity was 468.0 mg/g at 308 K, estimated from the Langmuir model. Furthermore, the modified peanut shell can be eluted easily using 3 mol/L NaOH. The proposed method was successfully applied to quantify the amount of SY in jelly and soft drinks with good recovery valuing from 98 to 104%. Hence, the proposed sensor shows a rapid and sensitive method, low cost, and simple, which is appropriate for alternative technique use for the analysis of food colorants in commercial products.
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页码:2158 / 2171
页数:13
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