Synthesis and structures of 5(3H)-oxotetrahydro-1H-imidazo[4,5-c][1,2,5]thiadiazole 2,2-dioxides

被引：0
|
作者：
G. A. Gazieva
A. N. Kravchenko
K. A. Lyssenko
R. G. Gaziev
O. V. Lebedev
N. N. Makhova
机构：
[1] Russian Academy of Sciences,N. D. Zelinsky Institute of Organic Chemistry
[2] Russian Academy of Sciences,A. N. Nesmeyanov Institute of Organoelement Compounds
来源：
Russian Chemical Bulletin | 2008年 / 57卷
关键词：
α-ureidoalkylation; 5(3; )-oxotetrahydro-1; -imidazo[4,5-; ][1,2,5]thiadiazole 2,2-dioxides; -(1,3-diethyl-5-hydroxy-2-oxoimidazolidin-4-yl)-; -dialkylsulfamides; X-ray diffraction study; conglomerate;
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摘要：
The reactions of sulfamides with 4,5-dihydroxyimidazolidin-2-ones were studied at ambient and high pressure. The previously unknown derivatives of 5(3H)-oxotetrahydro-1H-imidazo-[4,5-c][1,2,5]thiadiazole 2,2-dioxide, viz., sulfo analogs of tetrahydroimidazo[4,5-d]imidazole-2,5-(1H,3H) diones (glycolurils), were synthesized. The structures of some of these compounds were established by X-ray diffraction. The high-pressure reactions performed under conditions of solvent phase transitions afforded also N-(1,3-diethyl-5-hydroxy-2-oxoimidazolidin-4-yl)-N,N′-dialkylsulfamides. Among these compounds, a new conglomerate was found.
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页码：1744 / 1753
页数：9
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