Copper(II) complexes based on 2-thenoyltrifluoroacetone aroyl hydrazones: Synthesis, spectroscopy, and X-ray diffraction analysis

被引：0
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作者：
K. G. Avezov
B. B. Umarov
M. A. Tursunov
V. V. Minin
N. A. Parpiev
机构：
[1] Bukhara State University,Kurnakov Institute of General and Inorganic Chemistry
[2] Russian Academy of Sciences,undefined
来源：
Russian Journal of Coordination Chemistry | 2016年 / 42卷
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摘要：
Copper(II) complexes CuL • NH3 are synthesized by the interaction of ethanol solutions of parasubstituted 2-thenoyltrifluoroacetylmethane aroyl hydrazones (H2L1–H2L4) and an aqueous-ammonia solution of copper(II) acetate in an equimolar ratio. The copper(II) complexes are studied by elemental analysis, IR spectroscopy, and EPR spectroscopy. Single crystals of CuL3 • NH3 are grown from 1-(2-thenoyl)- 3,3,3-trifluoroacetone para-methylbenzoyl hydrazone and studied using X-ray diffraction analysis (CIF file CCDC 1045841).
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页码：470 / 475
页数：5
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