A Systematic Investigation of Long-Range Couplings in the 1H NMR Spectra of Dimeric Indanones

被引:0
|
作者
Susanne Felsinger
Hermann Kalchhauser
Horst Neudeck
机构
[1] Institute of Organic Chemistry,
[2] University of Vienna,undefined
[3] A-1090 Vienna,undefined
[4] Austria,undefined
关键词
Keywords. NMR spectroscopy; Indanones; Long-range couplings.;
D O I
暂无
中图分类号
学科分类号
摘要
 During the synthesis of methyl substituted indanones by intramolecular cyclization of 3-phenyl-propionic acids, dimerization led to by-products which can be considered as dimeric indanones. The proton NMR spectra of these compounds exhibit pronounced scalar couplings over up to seven bonds. A series of structures of the above type were investigated, and their NMR spectroscopic behaviour is discussed.
引用
收藏
页码:267 / 278
页数:11
相关论文
共 50 条
  • [1] A systematic investigation of long-range couplings in the 1H NMR spectra of dimeric indanones
    Felsinger, S
    Kalchhauser, H
    Neudeck, H
    MONATSHEFTE FUR CHEMIE, 2001, 132 (02): : 267 - 278
  • [2] LONG-RANGE COUPLINGS IN NMR SPECTRA OF ISOQUINOLINES
    BALKAU, F
    HEFFERNA.ML
    AUSTRALIAN JOURNAL OF CHEMISTRY, 1971, 24 (11) : 2311 - &
  • [3] LONG-RANGE COUPLINGS IN NMR SPECTRA OF ALKYL FORMATES
    DEKOWALEWSKI, DG
    KOWALEWSKI, VJ
    MOLECULAR PHYSICS, 1964, 8 (01) : 93 - &
  • [4] Long-Range Shielding Effects in the 1H NMR Spectra of Mosher-like Ester Derivatives
    Hoye, Thomas R.
    Erickson, Sara E.
    Erickson-Birkedahl, Sherrie L.
    Hale, Christopher R. H.
    Izgu, Enver Cagri
    Mayer, Michael J.
    Notz, Patrick K.
    Renner, Matthew K.
    ORGANIC LETTERS, 2010, 12 (08) : 1768 - 1771
  • [5] C-13 NMR SPECTRA AND LONG-RANGE C-13-H COUPLINGS IN SUBSTITUTED ETHYLENES
    CRECELY, KM
    CRECELY, RW
    GOLDSTEIN, JH
    JOURNAL OF MOLECULAR SPECTROSCOPY, 1971, 37 (02) : 252 - +
  • [6] Synthesis and total assignment of 1H and 13C NMR spectra of new oxoisoaporphines by long-range heteronuclear correlations
    Sobarzo-Sánchez, E
    De la Fuente, J
    Castedo, L
    MAGNETIC RESONANCE IN CHEMISTRY, 2005, 43 (12) : 1080 - 1083
  • [7] THE HIGHLY RESOLVED H-1-NMR SPECTRUM OF THIOANISOLE - PRECISE LONG-RANGE COUPLINGS TO THE METHYL PROTONS
    SCHAEFER, T
    BALEJA, JD
    JOURNAL OF MAGNETIC RESONANCE, 1984, 60 (01) : 131 - 135
  • [8] ANALYSIS OF H-1-NMR SPECTRA OF FLUORENE AND AZAFLUORENES - LONG-RANGE COUPLING-CONSTANTS
    FOMICHOV, AA
    LAWANIEDOGIAWERIE, SO
    PROSTAKOV, NS
    ORGANIC MAGNETIC RESONANCE, 1983, 21 (05): : 310 - 314
  • [9] A systematic investigation of carbamate stability constants by 1H NMR
    McCann, Nichola
    Duong Phan
    Fernandes, Debra
    Maeder, Marcel
    INTERNATIONAL JOURNAL OF GREENHOUSE GAS CONTROL, 2011, 5 (03) : 396 - 400
  • [10] LONG-RANGE EFFECTS IN PROTON NMR SPECTRA OF ALLENES
    MACOMBER, RS
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1971, (MAR-A): : 142 - &