Determination of iron and lead by flame atomic absorption spectrometry after preconcentration with sepiolite

被引:0
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作者
A. Rehber Türker
Hüseyin Bağ
Baki Erdoğan
机构
[1] Gazi Üniversitesi,Fen
[2] Kırıkkale Üniversitesi,Edebiyat Fakültesi
关键词
Sepiolite; Flame Atomic Absorption Spectrometry; Sodium Diethyldithiocarbamate; Hydrous Magnesium; Differential Thermal Analy;
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摘要
By using a new adsorbent (sepiolite) an adsorptionelution and atomic absorption spectrometric method has been developed for the preconcentration and determination of Fe and Pb. Recoveries of the analytes were 82 ± 3% for Fe and 91 ± 2% for Pb at 95% confidence level. For Cu it was only 5 ± 1%. The recovery of iron could be increased to about 97 ± 1% by complexing with EDTA, the recovery of copper only to 57 ± 2%. The optimised method was applied to the determination of lead in metal materials (e.g. brass).
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页码:351 / 353
页数:2
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