Synthesis of 5,6-O-Cyclohexylidene-1-amino-3-azahexane and Its Co(II), Ni(II), Cu(II) Complexes

被引：0

作者：

O. F. Ozturk

M. Sekerci

E. Ozdemir

机构：

[1] Canakkale Onsekiz Mart University,Faculty of Arts and Sciences, Chemistry Department

[2] Firat University,Faculty of Arts and Sciences, Chemistry Department

来源：

Russian Journal of Coordination Chemistry | 2005年 / 31卷

关键词：

Spectroscopy; Acetate; Physical Chemistry; Inorganic Chemistry; Magnetic Susceptibility;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

5,6-O-Cyclohexylidene-1-amino-3-azahexane (L) is synthesized from 1-chloro-2,3-O-cyclohexylidenepropane, which is prepared by the reaction between epichlorohydrin and cyclohexanone. In this reaction, BF3 · OEt2 is used as a catalyst. Complexes of Co(II), Ni(II) and Cu(II) acetates with this ligand are prepared. The structures of the ligand and its complexes are proposed based on elemental analysis, IR and UV-VIS spectroscopy, magnetic susceptibility, conductometry, and 1H and 13C NMR spectroscopy.

引用

页码：651 / 654

页数：3

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