Chemical Analysis of Hydroxyapatite Artificial Bone Powders by Energy Dispersive X-Ray Fluorescence Spectrometry (EDXRF)

被引:4
|
作者
Koksal, O. K. [1 ,2 ]
Apaydin, G. [1 ]
Cengiz, E. [1 ]
Samek, L. [2 ]
Karahan, I. H. [3 ]
Tozar, A. [3 ]
Lankosz, M. [2 ]
机构
[1] Karadeniz Tech Univ, Fac Sci, Dept Phys, TR-61080 Trabzon, Turkey
[2] AGH Univ Sci & Technol, Fac Phys & Appl Comp Sci, Dept Med Phys & Biophys, Krakow, Poland
[3] Mustafa Kemal Univ, Fac Sci & Literature, Dept Phys, Antakya, Turkey
关键词
EDXRF; X-ray Tube; Elemental analysis; Hydroxyapatite; COATINGS;
D O I
10.3964/j.issn.1000-0593(2018)08-2645-05
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
Stoichiometric hydroxyapatite (HA) nanoparticles were synthesized by a wet chemical method. Calcium nitrate tetra hydrate used as calcium source and dibasic ammonium phosphate used as phosphorous source. Calcium nitrate tetra hydrate and dibasic ammonium phosphate solutions were prepared by dissolving the salts in distilled water. Stoichiometric hydroxyapatite nanoparticles used by artificial bone powders and synthesized by a wet chemical method were analyzed using EDXRF method. The concentrations of K, Ca, Ti, V, Cr, Fe, Ni, Cu, Sr and Pb for artificial bone powders have been determined. Besides, Calcium contents were evaluated according to the agitation time and temperature in the production process.
引用
收藏
页码:2645 / 2649
页数:5
相关论文
共 42 条
  • [1] Adzila S, 2013, T TECH PUBL, V531
  • [2] Low-temperature crystallization and high-temperature instability of hydroxyapatite thin films deposited on Ru, Ti, and Pt metal substrates
    Akazawa, Housei
    Ueno, Yuko
    [J]. SURFACE & COATINGS TECHNOLOGY, 2015, 266 : 42 - 48
  • [3] Mechanism of calcium phosphate deposition in a hydrothermal coating process
    Asl, Sara Kaabi Falahieh
    Nemeth, Sandor
    Tan, Ming Jen
    [J]. SURFACE & COATINGS TECHNOLOGY, 2015, 270 : 197 - 205
  • [4] Barbosa M C, 2013, MAT SCI ENG C, V33, P5
  • [5] Bennett S C, 1983, J MATER SCI, V18, P11
  • [6] Chen Z F, 2004, ARCH ORAL BIOL, V49, P5
  • [7] Optimized Electrodeposition Concentrations for Hydroxyapatite Coatings on CoCrMo biomedical alloys by computational techniques
    Coskun, M. Ibrahim
    Karahan, Ismail H.
    Yucel, Yasin
    [J]. ELECTROCHIMICA ACTA, 2014, 150 : 46 - 54
  • [8] de Campos M, 2007, J MAT SCI MAT M, V18, P5
  • [9] Dorozhkin S V, 2007, J MATER SCI, V42, P4
  • [10] Bioceramics of calcium orthophosphates
    Dorozhkin, Sergey V.
    [J]. BIOMATERIALS, 2010, 31 (07) : 1465 - 1485