Synthesis and Crystal Structure of a New Macrocycle Based on Diethoxycarbonyl Glycoluril: C26H30N6O10

被引：0
|
作者：
Li Yi-Tao [1 ]
Zhu Yan-Ping [1 ]
Wu An-Xin [1 ]
机构：
[1] Cent China Normal Univ, Minist Educ, Key Lab Pesticide & Chem Biol, Wuhan 430079, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2009年 / 28卷 / 12期
基金：
中国国家自然科学基金;
关键词：
macrocycle; diethoxycarbonyl glycoluril; synthesis; crystal structure; BINDING;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A new macrocycle based on diethoxycarbonyl glycoluril 3, C26H30N6O10, has been synthesized and characterized by single-crystal X-ray diffraction. It crystallizes in monoclinic, space group P2(1)/c with a = 12.7291(10), b = 25.157(2), c = 8.5489(7) angstrom, beta = 104.4760(10)degrees, V= 2650.7(4) angstrom(3), Z = 4, C26H30N6O10, M-r = 586.56, F(000) = 1232, T = 292(2) K, D-c = 1.470 g/cm(3), mu = 0.115 mid I, the final R = 0.0590 and wR = 0.1299 for 4918 observed reflections with I > 2 sigma(I). In the structure of the title compound, a three-dimensional microporous architecture is formed via intermolecular hydrogen bonding interactions.
引用
收藏
页码：1593 / 1596
页数：4
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