tert-Butyl N-[6-(N,N-dipropylcarbamoyl)-1,3-benzothiazol-2-yl]carbamate

被引：3

作者：

Fang, Xin ^{[1
]}

Lei, Can ^{[1
]}

Yu, Hai-Yang ^{[1
]}

Huang, Ming-Dong ^{[2
]}

Wang, Jun-Dong ^{[1
]}

机构：

[1] Fuzhou Univ, Coll Chem & Chem Engn, Fuzhou 350108, Peoples R China

[2] Chinese Acad Sci, State Key Lab Struct Chem, Fujian Inst Res Struct Matter, Fuzhou 350002, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

BENZOTHIAZOLES;

D O I：

10.1107/S160053681001528X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound C(19)H(27)N(3)O(3)S, crystallizes with two unique molecules in the asymmetric unit. The benzene ring of each benzothiazole unit carries a dipropylcarbamoyl substituent in the 6-position and a tert-butyl carbamate unit on each thiazole ring. In the crystal structure, intermolecular N-H center dot center dot center dot N and weak C-H center dot center dot center dot O hydrogen bonds form centrosymmetric dimers. Additional C-H center dot center dot center dot O contacts construct a three-dimensional network. A very weak C-H center dot center dot center dot pi contact is also present.

引用

页码：O1239 / U1436

页数：14

共 50 条

[1] N-(1,3-Benzothiazol-2-yl)acetamide
Nayak, Prakash S.
Narayana, B.
Jasinski, Jerry P.
Yathirajan, H. S.
Kaur, Manpreet
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1622 - +
[2] tert-Butyl N-(thiophen-2-yl)carbamate
Hsu, Gene C.
Singer, Laci M.
Cordes, David B.
Findlater, Michael
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1413 - +
[3] tert-butyl N-{2-[N-(N,N′-dicyclohexylureidocarbonylethyl)carbamoyl]prop-2-yl}carbamate
Banerjee, R
Maji, SK
Banerjee, A
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2000, 56 (09): : 1120 - 1121
[4] tert-butyl N-(phosphinoyloxy) carbamate
Blatch, Alexandrea J.
Howard, Judith A. K.
Probert, Michael R.
Smethurst, Christian A.
Whiting, Andrew
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O5346 - O5348
[5] N-(1,3-benzothiazol-2-yl)-4-(dimethylamino)-benzylamine
Saraçoglu, H
Çaliskan, N
Davran, C
Soylu, S
Bati, H
Büyükgüngör, O
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O2090 - O2092
[6] Antidiabetic activity of N-(6-substituted-1,3-benzothiazol-2-yl)benzenesulfonamides
Moreno-Diaz, Hermenegilda
Villalobos-Molina, Rafael
Ortiz-Andrade, Rolffy
Diaz-Coutino, Daniel
Medina-Franco, Jose Luis
Webster, Scott P.
Binnie, Margaret
Estrada-Soto, Samuel
Ibarra-Barajas, Maximiliano
Leon-Rivera, Ismael
Navarrete-Vazquez, Gabriel
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2008, 18 (09) : 2871 - 2877
[7] 2-(Adamantan-1-yl)-N-(6-methoxy-1,3-benzothiazol-2-yl)acetamide
Bunev, Alexander S.
Sklyuev, Prokofij V.
Ostapenko, Gennady I.
Purygin, Petr P.
Khrustalev, Victor N.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1472 - +
[8] Synthesis and heterocyclization of N-[4-(1,3-benzothiazol-2-yl)phenyl]-β-alanines
Rutkauskas, Kestutis
Tumosiene, Ingrida
Kantminiene, Kristina
Beresnevicius, Zigmuntas J.
CHEMIJA, 2012, 23 (04): : 312 - 321
[9] tert-Butyl N-[(S)-1-hydrazinecarbonyl-2-hydroxyethyl]carbamate
Pinheiro, Alessandra C.
de Souza, Marcus V. N.
Wardell, Solange M. S. V.
Wardell, James L.
Tiekink, Edward R. T.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O994 - U3669
[10] Crystal structure of N,N,N-tris[(1,3-benzothiazol-2-yl)methyl]amine
Mdluli, Velabo
Golen, James A.
Rheingold, Arnold L.
Manke, David R.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O786 - U562

← 1 2 3 4 5 →