A new 1,2,3,4-tetrahydroquinoxaline derivative combining baicalein and 1,2-diphenylethylenediamine moieties: Structure and its fluorescence-based detection of nitroaromatics

被引：5

作者：

Fu, Qiang ^{[1
]}

Zhang, Yao ^{[1
]}

Liu, Baokai

Guo, Fang ^{[1
]}

机构：

[1] Liaoning Univ, Coll Chem, Shenyang 110036, Liaoning, Peoples R China

来源：

JOURNAL OF MOLECULAR STRUCTURE | 2018年 / 1171卷

基金：

美国国家科学基金会;

关键词：

1,2,3,4-tetrahydroquinoxaline derivative; Baicalein; 1,2-diphenylethylenediamine; Fluorescence detection; ASYMMETRIC HYDROGENATION; ENANTIOSELECTIVE REDUCTION; CRYSTAL-STRUCTURE; C-N; QUINOXALINES; EFFICIENT; ROUTE; NITROBENZENE; EXPLOSIVES; GROWTH;

D O I：

10.1016/j.molstruc.2018.05.089

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A new heterocyclic 1,2,3,4-tetrahydroquinoxaline derivative compound, named as (2R,3R)-5-hydroxy2,3,8-tripheny1-3,4-dihydro-1H-pyrano[3,2-f]quinoxalin-10(2H)-one (A) has been obtanied from baicalein and 1,2,3,4-tetrahydroquinoxaline through a new and relatively straightforward crystallization approach. The compound A has been characterialzed by IR, H-1 NMR, TGA and X-ray crystallography. The compound shows good photolumicent property and the ability to detect trace amounts of nitrobenzene, 2-nitrotoluene and 3-nitrotoluene. (C) 2018 Elsevier B.V. All rights reserved.

引用

页码：69 / 75

页数：7

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