A three-dimensional electron spin resonance microscope

被引：18
|
作者：
Blank, A [1 ]
Dunnam, CR [1 ]
Borbat, PP [1 ]
Freed, JH [1 ]
机构：
[1] Cornell Univ, Natl Biomed Ctr Adv ESR Technol, Dept Chem & Chem Biol, Ithaca, NY 14853 USA
来源：
REVIEW OF SCIENTIFIC INSTRUMENTS | 2004年 / 75卷 / 09期
关键词：
D O I：
10.1063/1.1786353
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
An electron spin resonance (ESR) imaging system, capable of acquiring three-dimensional (3D) images with a resolution of similar to10 X 10 X 30 mum in a few minutes of acquisition, is presented. This ESR microscope employs a commercial continuous wave ESR spectrometer, working at 9.1 GHz, in conjunction with a miniature imaging probe (resonator+gradient coils), gradient current drivers, and control software. The system can acquire the image of a small (similar to1.5 X 1.5 X 0.25 mm) sample either by the modulated field gradient method, the projection reconstruction method, or by a combination of the two. A short discussion regarding the resolution of the modulated field gradient method in two-dimensional (2D) and 3D imaging is given. Detailed descriptions of the various system components are provided, along with several examples of 2D and 3D images that demonstrate the capabilities of the system. (C) 2004 American Institute of Physics.
引用
收藏
页码：3050 / 3061
页数：12
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