Synthesis and characterization of novel polyamides based on tridecanedioic acid: Nylons 3 13, 5 13, 6 13, 7 13, 9 13, 10 13, 11 13

被引：0
|
作者：
Cui, XW [1 ]
Yan, DY [1 ]
Xiao, D [1 ]
机构：
[1] Shanghai Jiao Tong Univ, Coll Chem & Chem Technol, Shanghai 200240, Peoples R China
来源：
E-POLYMERS | 2004年
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D O I：
暂无
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Linear polyamides with high aliphatic content were prepared through step-heating melt polycondensation of tridecanedioic acid with various diamines. The synthesized polyamides were characterized comprehensively by means of IR, NIVIR and Raman spectroscopy. In addition, thermogravimetry, differential scanning calorimetry and dynamic mechanical analysis were used to investigate thermal properties of the obtained polyamides. It was found that melting and crystallization temperatures decrease as the aliphatic content increases. X-ray diffraction was applied to determine the crystal structures of the polyamides.
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页数：9
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