N-[Bis(benzylamino)phosphoryl]-2,2,2-trichloroacetamide

被引：3
|
作者：
Ovchynnikov, Vladimir A. [1 ]
机构：
[1] Natl Taras Shevchenko Univ, Dept Chem, UA-01033 Kiev, Ukraine
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
CRYSTAL; ACID;
D O I：
10.1107/S1600536810017873
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C(16)H(17)Cl(3)N(3)O(2)P, the P atom has a slightly distorted tetrahedral configuration. The conformations of the carbonyl and phosphoryl groups are anti to each other. In the crystal, intermolecular N-H center dot center dot center dot O hydrogen bonds link the molecules into infinite chains parallel to the b axis.
引用
收藏
页码：O1425 / U1560
页数：10
相关论文
共 50 条
  • [1] N-{Bis[methyl(phenyl)amino]phosphoryl}-2,2,2-trichloroacetamide
    Znovjyak, Kateryna O.
    Ovchynnikov, Vladimir A.
    Sliva, Tetyana Yu.
    Shishkina, Svitlana V.
    Amirkhanov, Vladimir M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2812 - U1371
  • [2] SYNTHESIS AND CRYSTAL STRUCTURE OF NEW Zn(II) COMPLEX WITH N-[BIS(BENZYLAMINO)PHOSPHORYL]-2,2,2-TRICHLOROACETAMIDE
    Zozulia, Valeriia
    Ovchynnikov, Vladimir
    Slyva, Tetiana
    Rusanova, Julia
    Amirkhanov, Volodymyr
    CHEMISTRY JOURNAL OF MOLDOVA, 2021, 16 (02): : 58 - 65
  • [3] Bis(N-{bis[methyl(phenyl)amino]phosphoryl}-2,2,2-trichloroacetamide) dinitratodioxidouranium(VI)
    Znovjyak, Kateryna O.
    Ovchynnikov, Vladimir A.
    Sliva, Tetyana Yu.
    Shishkina, Svitlana V.
    Amirkhanov, Vladimir M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M306 - U3613
  • [4] N-[Bis(dimethylamino)phosphinoyl]-2,2,2-trichloroacetamide
    Amirkhanov, Oleksiy V.
    Moroz, Olesia V.
    Znovjyak, Kateryna O.
    Trush, Elizaveta A.
    Sliva, Tetyana Yu.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1102 - U331
  • [5] Bis{N-[bis(pyrrolidin-1-yl)phosphoryl]-2,2,2-trichloroacetamide}dinitratodioxidouranium(VI)
    Znovjyak, Kateryna O.
    Ovchynnikov, Vladimir A.
    Moroz, Olesia V.
    Shishkina, Svitlana V.
    Amirkhanov, Vladimir M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M322 - U3749
  • [6] Tris{N-[bis(pyrrolidin-1-yl)phosphoryl]-2,2,2-trichloroacetamide}trichloridoerbium(III)
    Znovjyak, Kateryna O.
    Ovchynnikov, Vladimir A.
    Shishkina, Svitlana V.
    Sliva, Tetyana Yu.
    Amirkhanov, Vladimir M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M447 - U1014
  • [7] Crystal structures of N-(4-methyl phenyl)-2,2,2-trichloroacetamide, N-(2,3-dimethyl phenyl)-2,2,2-trichloroacetamide and N-(2-nitro phenyl)-2,2,2-trichloroacetamide
    Dou, SQ
    Fuess, H
    Weiss, A
    Gowda, BT
    Krishnan, VG
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1997, 212 (07): : 532 - 537
  • [8] Copper(II) complexes based on N-(bis(diethylamino)phosphoryl)-2,2,2-trichloroacetamide with pyridine and 4,4′-bipyridine
    Ovchynnikov, Vladimir
    Gubina, Kateryna
    Shatrava, Yuliia
    Dyakonenko, Viktoriya
    Konovalova, Irina
    Shishkina, Svitlana
    Amirkhanov, Vladimir
    JOURNAL OF COORDINATION CHEMISTRY, 2022, 75 (1-2) : 61 - 69
  • [9] THE BOND N-CL - CRYSTAL-STRUCTURES AND CL-35 NQR OF N-CHLORO-N-PHENYL-2-CHLOROACETAMIDE, N-CHLORO-N-PHENYL-2,2-DICHLOROACETAMIDE, N-CHLORO-N-PHENYL-2,2,2-TRICHLOROACETAMIDE, AND N-PHENYL-2,2,2-TRICHLOROACETAMIDE
    DOU, SQ
    GOWDA, BT
    PAULUS, H
    WEISS, A
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION A-A JOURNAL OF PHYSICAL SCIENCES, 1994, 49 (12): : 1136 - 1144
  • [10] PREPARATION AND HPLC CHARACTERIZATION OF 3-(2,2,2-TRICHLOROACETAMIDE)PROPYLSILANE AND 3-(2,2,2-TRICHLOROETHOXY)PROPYLSILANE BONDED PHASES
    PHARR, DY
    UDEN, PC
    SIGGIA, S
    JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1988, 26 (09) : 432 - 438
12345