(E)-5-(3,5-Dimethylphenyl)-N-[4-(methylsulfanyl)benzylidene]-1,3,4-thiadiazol-2-amine

被引：2
|
作者：
Hu, Jun [1 ]
Ji, Jin-xiu [2 ]
Zhou, Ying [3 ]
Wang, Ji-kui [4 ]
Xu, Yan-hua [1 ]
机构：
[1] Nanjing Univ Technol, Dept Safety Engn, Coll Urban Construct & Safety Engn, Nanjing 210009, Peoples R China
[2] Sinochem Jiangsu Corp, Ctr Res & Dev, Nanjing 210002, Peoples R China
[3] Nanjing Univ Technol, Dept Environm Engn, Coll Environm, Nanjing 210009, Peoples R China
[4] Nanjing Univ Technol, Dept Appl Chem, Coll Sci, Nanjing 210009, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
Data-to-parameter ratio = 14.8; Mean σ(C-C) = 0.007 Å; R factor = 0.065; Single-crystal X-ray study; T = 298 K; WR factor = 0.208;
D O I：
10.1107/S1600536810001558
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C(18)H(17)N(3)S(2), was synthesized by the reaction of 5-(3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine and 4-(methylsulfanyl) benzaldehyde. An intramolecular C-H center dot center dot center dot S hydrogen bond results in the formation of a planar (r.m.s. deviation = 0.003 angstrom) five-membered ring. In the crystal structure, intermolecular C-H center dot center dot center dot N hydrogen bonds link the molecules to form layers parallel to (011).
引用
收藏
页码：O410 / U2924
页数：10
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