A low-cost upgrade of a commercial magnetic resonance spectrometer to a broad-band system for NMR and ESR

被引:3
|
作者
Rösch, P [1 ]
Kelemen, MT [1 ]
Wokrina, T [1 ]
Dormann, E [1 ]
机构
[1] Univ Karlsruhe, TH, Inst Phys, D-76128 Karlsruhe, Germany
关键词
magnetically ordered compounds; one-dimensional conductors; frequency range extension; frequency mixing; untuned coils; short pulses; broad-band NMR; pulsed rf ESR; NMR signal calibration;
D O I
10.1088/0957-0233/11/11/310
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Due to their longevity and availability pulsed magnetic resonance spectrometers of the types Bruker CXP and Bruker MSL are widely used in research institutions. This contribution gives a detailed description of how to extend these spectrometers to broad-band systems for NMR and ESR measurements. As it is based on off-the-shelf components, the approach reported here is both cost and time effective. Experimental results for a magnetically ordered intermetallic compound and a one-dimensional organic conductor demonstrate the performance of the system. Particular attention is paid to the calibration procedure.
引用
收藏
页码:1610 / 1616
页数:7
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