An efficient and convenient procedure for the synthesis of 2-alkyl-2-alkoxy-1,2-di(furan-2-yl)ethanone under ultrasound in the presence of solid-liquid phase transfer catalysis conditions

被引:4
|
作者
Zhang, Feng
Sun, Jikui
Gao, Dawei
Li, Yazhuo
Zhang, Yumin
Zhao, Tianqi
Chen, Xiaodong
机构
[1] Jilin Univ, Coll Chem, Changchun 130012, Peoples R China
[2] Jilin Univ, Expt Ctr Testing Sci, Changchun 130023, Peoples R China
关键词
ultrasound; phase transfer catalysis; alkyl halides; furoin; alkylation;
D O I
10.1016/j.ultsonch.2007.02.004
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
Irradiation with ultrasound is found to facilitate the synthesis of 2-alkyl-2- alkoxy-1, 2-di(furan-2-yl)ethanone in the presence of tetrabutylammonium bromide (TBAB) as solid-liquid phase transfer catalysis. A higher yields (> 70%) and shorter reaction time (< 15 min) give this method obvious advantages over the conventional ones. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:493 / 496
页数:4
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