2,7-di-tert-butyl-9,9-dimethyl-4,5-bis(4-tritylanilinocarbonyl)-9H-xanthene methanol trisolvate monohydrate

被引:0
|
作者
Vysotsky, Myroslav O. [1 ]
Schollmeyer, Dieter [1 ]
机构
[1] Univ Mainz, Fachbereich Chem Pharm & Geowissensch, D-55128 Mainz, Germany
关键词
D O I
10.1107/S1600536806051439
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C75H68N2O3 center dot 3CH(3)OH center dot H2O, was synthesized starting from the corresponding acid and p-tritylaniline. Single crystals were obtained from a methanol solution as a solvate, with three methanol molecules and one water molecule. The solid-state structure proves the existence of an intramolecular bifurcated hydrogen bond between one amide H atom and the carbonyl and xanthene O atoms. The packing is stabilized by intermolecular hydrogen bonds.
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页码:O169 / O171
页数:3
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