Synthesis of Methacrylate-Containing Oligosilsesquioxanes via Acidic Hydrolytic Polycondensation in the Medium of Methacrylate Monomers

被引：7

作者：

Bredov, N. S. ^{[1
]}

Soan, Le Phu ^{[1
]}

Kireev, V. V. ^{[1
]}

Bykovskaya, A. A. ^{[1
]}

Sokol'skaya, I. B. ^{[2
]}

Gorlov, M. V. ^{[1
]}

Esin, A. S. ^{[1
]}

Bekmukhamedova, S. R. ^{[1
]}

Polyakov, V. A. ^{[1
]}

机构：

[1] Mendeleev Univ Chem Technol, Miusskaya Pl 9, Moscow 125047, Russia

[2] State Res Inst Chem & Technol Organoelement Cpds, Sh Entuziastov 38, Moscow 111123, Russia

来源：

POLYMER SCIENCE SERIES B | 2017年 / 59卷 / 03期

关键词：

PARTIAL ACIDOLYSIS; MASS-SPECTROMETRY; OLIGOORGANOSILSESQUIOXANES;

D O I：

10.1134/S1560090417030022

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

Methacrylate-containing oligosilsesquioxanes with a molecular mass of 700-4000 are synthesized via the acidic hydrolytic polycondensation of gamma-methacryloxy-propyltrimethoxysilane (A-174) in the medium of methyl methacrylate or in a mixture of bis(methacrylates). The structure of the oligomers is studied by (1)De and Si-29 NMR spectroscopy and MALDI-TOF mass spectrometry.

引用

页码：240 / 247

页数：8

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