(R,S)-methyl 3-methyl-5-oxo-1-phenylcyclo-hex-3-ene-1-carboxylate

被引:2
|
作者
Yao, Li-Ying [1 ]
Zhang, Chen [1 ]
Wang, Bi-Song [1 ]
机构
[1] Zhejiang Univ, Dept Med Chem, Coll Pharmaceut Sci, Hangzhou 310031, Zhejiang, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2006年 / 62卷
关键词
D O I
10.1107/S1600536806021441
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C15H16O3, has two molecules in the asymmetric unit. The cyclohex-2-enone ring has an envelope conformation in both molecules. The crystal exhibits twinning. The molecular packing in the crystal structure is determined by weak intermolecular C-H center dot center dot center dot O interactions.
引用
收藏
页码:O2768 / O2769
页数:2
相关论文
共 50 条
  • [1] PREPARATION AND DETERMINATION OF THE OPTICAL PURITY OF S-3-METHYL-PENT-1-ENE AND S-4-METHYL-HEX-1-ENE
    PINO, P
    LARDICCI, L
    CHEMISTRY & INDUSTRY, 1959, (15) : 483 - 484
  • [2] SYNTHESIS OF METHYL 5-HYDROXY-2METHYL-3-OXO-1-CYCLOPENTENE-1-CARBOXYLATE - METHYL ESTER OF A PICROTOXININ DEGRADATION PRODUCT
    FINCH, N
    SCHLITTLER, E
    TETRAHEDRON, 1968, 24 (15) : 5421 - +
  • [3] Optimization of the production of methyl 1,3,4-trimethylcyclohex-3-ene-1-carboxylate
    Marshalok, Halyna
    Kostiv, Iryna
    Polyuzhin, Ihor
    Marshalok, Olha
    Vytrykush, Nataliya
    PRZEMYSL CHEMICZNY, 2016, 95 (04): : 745 - 750
  • [4] Synthesis of Methyl 2-Bromo-3-oxocyclopent-1-ene-1-carboxylate
    Tata, Rama Rao
    Harmata, Michael
    ORGANIC SYNTHESES, 2018, 95 : 425 - +
  • [5] Methyl 6-methyl-1-oxo-2,3,4,9-tetrahydrocarbazole2-carboxylate
    Gunaseelan, A. Thomas
    Thiruvalluvar, A.
    Martin, A. Ebenezer
    Prasad, K. J. Rajendra
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2413 - U759
  • [6] Asymmetric synthesis of pent-3-yl (R)-6-methyl-cyclohex-1-ene carboxylate
    Garrido, Narciso M.
    Diez, David
    Dominguez, Sara H.
    Garcia, Mercedes
    Sanchez, M. Rosa
    Davies, Stephen G.
    TETRAHEDRON-ASYMMETRY, 2006, 17 (15) : 2183 - 2186
  • [7] Methyl 8-hydroxy-(S)-3-methyl-1-oxoisochromane-5-carboxylate (5-methoxycarbonylmellein)
    Wang, JF
    Zhang, YJ
    Huang, YJ
    Su, WJ
    Lu, Y
    Zhao, YF
    Ng, SW
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1233 - O1234
  • [8] Improved synthesis of methyl 3-oxo-2,6,6-trimethylcyclohex-1-ene-1-carboxylate, an A-ring intermediate for (±)strigol
    Qianchao
    Pi, Shiqing
    Chen, Xinzhi
    JOURNAL OF CHEMICAL RESEARCH, 2007, (08) : 494 - 496
  • [9] Methyl 9-methyl-1-oxo-2,3,4,9-tetrahydro-1H-carbazole-2-carboxylate
    Thiruvalluvar, A.
    Gunaseelan, A. Thomas
    Martin, A. Ebenezer
    Prasad, K. J. Rajendra
    Butcher, R. J.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3093 - U2492
  • [10] trans-(1R,3S)-methyl 1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate
    Alam, Samina
    Hasan, Mashooda
    Saeed, Sadaf
    Fischer, Andreas
    Khan, Naeema
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O871 - O872