Crystal structure of triethylentetraammonium bis monohydrogenmonophosphate dihydrate, [NH3(CH2)2NH2(CH2)2NH2(CH2)2NH3](HPO4)2•2H2O

被引：10
|
作者：
Elaoud, Z
Kamoun, S
Mhiri, T [1 ]
Jaud, J
机构：
[1] Fac Sci Sfax, Dept Chim, Lab Etat Solide, Sfax 3038, Tunisia
[2] ENIS, Lab Cristallochim Solide, Sfax 3038, Tunisia
[3] CNRS, Ctr Elaborat Mat & Etud Struct, F-31055 Toulouse, France
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 1999年 / 29卷 / 05期
关键词：
organic phosphate; structure;
D O I：
10.1023/A:1009588517216
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The salt triethylentetraammonium bis monohydrogenmonophosphate dihydrate is monoclinic with the following unit cell dimensions: a = 8.462(1), b = 10.500(1), c = 9.520 Angstrom, beta = 99.297(1)degrees space group P2(1)/n with Z = 2. The structure was solved by the Patterson method and refined to final R value of 0.043 for 1590 independent reflections. The structure consists of infinite parallel two-dimensional [(1) over bar 01] planes built of mutually connected ions and water molecules by strong O-H ... O and N-H ... O hydrogen bonding.
引用
收藏
页码：541 / 545
页数：5
相关论文
共 50 条
  • [1] Crystal structure of triethylentetraammonium bis monohydrogenmonophosphate dihydrate, [NH3(CH2)2NH2(CH2)2NH2(CH2)2NH3](HPO4)2 · 2H2O
    Zakaria Elaoud
    Slaheddine Kamoun
    Tahar Mhiri
    Joel Jaud
    Journal of Chemical Crystallography, 1999, 29 : 541 - 545
  • [2] Crystal structure of triethylentetraammonium bis monohydrogen-monophosphate dihydrate β-NH3(CH2)2NH2(CH2)2NH2(CH2)2NH3(HPO4)2·2H2O
    Z. Elaoud
    S. Kamoun
    T. Mhiri
    Journal of Chemical Crystallography, 1999, 29 : 1287 - 1290
  • [3] Crystal structure of triethylentetraammonium bis monohydrogen-monophosphate dihydrate β-NH3(CH2)2NH2(CH2)2NH2(CH2)2NH3(HPO4)2•2H2O
    Elaoud, Z
    Kamoun, S
    Mhiri, T
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 1999, 29 (12) : 1287 - 1290
  • [4] SynthesisandCharacterizationof[NH3（CH2）2NH2（CH2）2NH3]BiCl6
    徐刚
    付明来
    蔡丽珍
    张章静
    郭国聪
    黄锦顺
    结构化学, 2006, (03) : 338 - 342
  • [5] Synthesis and Characterization of [NH3(CH2)2NH2(CH2)2NH3]BiCl6
    徐刚
    付明来
    蔡丽珍
    张章静
    郭国聪
    黄锦顺
    Chinese Journal of Structural Chemistry, 2006, (03) : 338 - 342
  • [6] Synthesis and characterization of [NH3(CH2)2NH2(CH2)2NH3]BiCl6
    Xu, G
    Fu, ML
    Cai, LZ
    Zhang, ZJ
    Guo, GC
    Huang, JS
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2006, 25 (03) : 338 - 342
  • [7] Crystal structure of bis(triethylenetetramine) tris(zirconium) hexa(nitrilotriacetate) tetrahydrate, (NH3(CH2)2NH(CH2)2NH2(CH2)2NH3)2(Zr)3(N(CH2COO)3)6 • 4H2O
    Haussühl, E
    Haussühl, S
    Schreuer, J
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2000, 215 (01): : 98 - 100
  • [8] CHEMICAL PREPARATIONS, MAIN CRYSTALLOGRAPHIC AND STRUCTURAL FEATURES OF 2 NEW MONOPHOSPHATES - [NH3(CH2)3NH3] HPO4 H2O AND [NH3(CH2)2NH(CH2)2NH3].HPO4.2H2O
    KAMOUN, S
    JOUINI, A
    DAOUD, A
    COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II, 1990, 310 (06): : 733 - 738
  • [9] Synthesis of a layered zinc phosphate, [NH3(CH2)2NH2( CH2)3NH3][Zn2(PO4)(HPO4)2]•H2O, and its transformation to a extra-large pore three-dimensional zinc phosphate, [NH3(CH2)2NH2(CH2)3NH3][Zn3(PO4)(HPO4)3]
    Natarajan, S
    CHEMICAL COMMUNICATIONS, 2002, (07) : 780 - 781
  • [10] Solvothermal Synthesis and Crystal Structure of [H2N（CH2）2NH3]{Co[H2N（CH2）2NH2]3}[SbSe4]
    FU Ming-Lai a
    结构化学, 2004, (07) : 731 - 734
12345