One-pot multicomponent synthesis hexahydroquinoline derivatives in Triton X-100 aqueous micellar media

被引：13
|
作者：
Heravi, Mohammad Reza Poor [1 ]
Mehranfar, Shadi [1 ]
Shabani, Nemat [1 ]
机构：
[1] Payame Noor Univ, Dept Chem, Tehran 193954697, Iran
来源：
COMPTES RENDUS CHIMIE | 2014年 / 17卷 / 02期
关键词：
Multicomponent reactions (MCRs); One-pot reaction; Hexahydroquinolines; Triton X-100; Non-ionic surfactant; Dimedone; POLYHYDROQUINOLINE DERIVATIVES; EFFICIENT SYNTHESIS; HANTZSCH REACTION; CATALYZED FACILE; AMMONIUM-NITRATE; 1,4-DIHYDROPYRIDINES; ESTERS; ACID;
D O I：
10.1016/j.crci.2012.11.017
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A facile and efficient synthesis of hexahydroquinoline derivatives (5a-o) was reported via a four-component condensation reaction of aldehydes, dimedone, methyl aceto acetate and ammonium acetate in the presence of Triton X-100 in water at room temperature. The use of just 20 mol % of Triton X-100 in water solvent is sufficient. The FT-IR, F-19 NMR, H-1 NMR, C-13 NMR spectra and elemental analysis confirm the structure of the compounds. (c) 2012 Academie des sciences. Published by Elsevier Masson SAS. All rights reserved.
引用
收藏
页码：141 / 145
页数：5
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