Synthesis of Fe-SiC Nanowires via Precursor Route

被引：20
|
作者：
Mishra, R. [1 ]
Tiwari, R. K. [1 ]
Saxena, A. K. [1 ]
机构：
[1] Def Mat & Stores Res & Dev Estab, Kanpur 208013, Uttar Pradesh, India
来源：
JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS | 2009年 / 19卷 / 02期
关键词：
Polycarbosilane; Iron polycarbosilane; Fe-SiC; Nano SiC wire; SILICON-CARBIDE NANORODS; OPTICAL-PROPERTIES; POLYCARBOSILANE; PYROLYSIS; NANOTUBES; CERAMICS; POLYMERS;
D O I：
10.1007/s10904-009-9259-7
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Magnetic SiC nanowires were obtained by the pyrolysis of iron containing polycarbosilane (PCS) which in turn was synthesized by the reaction of polycarbosilane and iron (III) acetylacetonate [Fe(acac)(3)] in solvent. Characterization of synthesized polycarbosilane and Fe-SiC were performed with Fourier transformation infrared spectroscopy, energy dispersive X-ray spectrometry, powder X-ray diffraction, thermogravimetric analysis, scanning electron microscopy, electron spin resonance and vibrating sample magnetometer.
引用
收藏
页码：223 / 227
页数：5
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