Synthesis, crystal structure and spectroscopic properties of a novel tricyclic cinnoline derivative

被引：1
|
作者：
Yuan, Yuehua [1 ]
Tian, Maozhong [1 ]
Yin, Qiangfeng [2 ]
Feng, Feng [1 ]
机构：
[1] Shanxi Datong Univ, Coll Chem & Environm Engn, Datong 037009, Peoples R China
[2] East China Univ Sci & Technol, Chem Engn Inst, Prod Engn Dept, Shanghai 200237, Peoples R China
来源：
DYES AND PIGMENTS | 2017年 / 141卷
基金：
美国国家科学基金会;
关键词：
Cinnoline derivative; Synthesis; Absorption spectra; Fluorescence quantum yields; Single crystal; Hydrogen bond; PROTOCOL; IONS;
D O I：
10.1016/j.dyepig.2017.02.038
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
A facile, efficient synthesis of the novel cinnoline derivative (E)-2,2'-(3-((3-bromophenyl) imino)-5-(tertbutyl)-3H-pyrrolo[3,2,1-fi]cinnoline-2,8-diy1)bis(propan-an-2-01) (1) is reported. Richter cyclization of an o-ethynenearyldiazonium salt gave the cinnoline derivative which underwent a cyclization reaction to form the unexpected tricyclic compound 1. The absorption and fluorescence properties of cinnoline 1 were investigated in various solvents. A single crystal of 1 was grown and analyzed by X-ray diffraction analysis. The results showed that the inclusion compound was formed between the host (cinnoline 1) and the guest (acetone) in the crystal. (C) 2017 Elsevier Ltd. All rights reserved.
引用
收藏
页码：363 / 365
页数：3
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