One-pot two-step approach to selenides.: Phase-transfer catalyzed synthesis of ω-hydroxyalkyl selenides

被引：3
|
作者：
Hu, XB [1 ]
Tian, ZJ [1 ]
Chen, YY [1 ]
Lu, XR [1 ]
机构：
[1] Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2000年 / 30卷 / 03期
关键词：
D O I：
10.1080/00397910008087348
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
omega-hydroxyalkyl selenides were synthesized in good yields under phase-transfer conditions which involved hadrazine reduction on selenium powder and then alkylation with omega-haloalkyl alcohols in the presence of TBAB, reduction the resulting diselenides with KBH4 followed by treatment with alkyl halides.
引用
收藏
页码：523 / 529
页数：7
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